Technology Process of C24H32N4O5
There total 3 articles about C24H32N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
O-(benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate; triethylamine;
In
dichloromethane;
at 25 ℃;
for 5h;
DOI:10.2174/092986610791306661
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / tetrahydrofuran; water / 12 h / 0 °C
2: O-(benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate; triethylamine / dichloromethane / 5 h / 25 °C
With
O-(benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.2174/092986610791306661
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; copper (II) carbonate hydroxide / water / 2 h / 80 - 90 °C
1.2: 12 h / 25 °C
1.3: 24 h / 25 °C
2.1: sodium hydroxide / tetrahydrofuran; water / 12 h / 0 °C
3.1: O-(benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate; triethylamine / dichloromethane / 5 h / 25 °C
With
hydrogenchloride; copper (II) carbonate hydroxide; O-(benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.2174/092986610791306661