C₂₆H₃₄N₂O₄

Base Information

• Chemical Name: C₂₆H₃₄N₂O₄
• CAS No.: 1340548-50-6
• Molecular Formula: C₂₆H₃₄N₂O₄
• Molecular Weight: 438.567
• Mol file: 1340548-50-6.mol

Synonyms:

Chemical Property of C₂₆H₃₄N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₄N₂O₄

There total 9 articles about C₂₆H₃₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H38O4Si (1340548-92-6) → C26H34N2O4 (1340548-50-6)

Guidance literature:

Multi-step reaction with 8 steps

1: pyridine / methanol / Inert atmosphere

2: copper(l) iodide; lithium bromide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / methanol / Inert atmosphere

4: triethylamine / dichloromethane / Inert atmosphere

5: sodium hydride / tetrahydrofuran / Inert atmosphere

6: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

7: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

8: methanol / Inert atmosphere

With pyridine; copper(l) iodide; oxalyl dichloride; tetrabutyl ammonium fluoride; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; lithium bromide; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1021/ja207591e

Reference yield:

C34H46O5Si (1340548-98-2) → C26H34N2O4 (1340548-50-6)

Guidance literature:

Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

3: methanol / Inert atmosphere

With oxalyl dichloride; tetrabutyl ammonium fluoride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1021/ja207591e

Reference yield:

C24H32O2Si (1340548-96-0) → C26H34N2O4 (1340548-50-6)

Guidance literature:

Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / Inert atmosphere

2: sodium hydride / tetrahydrofuran / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / Inert atmosphere

4: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

5: methanol / Inert atmosphere

With oxalyl dichloride; tetrabutyl ammonium fluoride; sodium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1021/ja207591e

upstream raw materials:

C₂₈H₃₈O₄Si

C₂₄H₃₂O₂Si

C₂₉H₄₀O₃Si

C₃₄H₄₆O₅Si