cis/trans-3)(PPh₃)2>

Base Information

• Chemical Name: cis/trans-3)(PPh₃)2>
• CAS No.: 66807-76-9
• Molecular Formula: C₃₆H₃₀Cl₄P₂PdSn
• Molecular Weight: 891.524
• Mol file: 66807-76-9.mol

Synonyms:

Chemical Property of cis/trans-3)(PPh₃)2>

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis/trans-3)(PPh₃)2>

There total 2 articles about cis/trans-3)(PPh₃)2> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

dichloro bis(acetonitrile) palladium(II) (21264-30-2,90243-59-7,14592-56-4) + triphenylphosphine (603-35-0) + tin(ll) chloride → cis/trans-3)(PPh3)2> (23507-89-3,66807-76-9,66807-81-6)

Guidance literature:

In dichloromethane; acetone; to soln. PPh3 in CH2Cl2 soln. SnCl2 in acetone was added, Pd complex wasadded, stirred for 10 min; petroleum ether was added, stirred for 10 min, ppt. was filtered, washedwith petroleum ether and dried in vacuo; elem. anal.;

DOI:10.1039/c2ob25275a

Reference yield:

trans-bis(triphenylphosphine)palladium dichloride (28966-81-6) + tin(ll) chloride → cis/trans-3)(PPh3)2> (23507-89-3,66807-76-9,66807-81-6)

Guidance literature:

In toluene; under N2;

upstream raw materials:

trans-bis(triphenylphosphine)palladium dichloride

dichloro bis(acetonitrile) palladium(II)

triphenylphosphine