3-cyano-4-methylbenzene-1-sulfonyl chloride

Base Information

• Chemical Name: 3-cyano-4-methylbenzene-1-sulfonyl chloride
• CAS No.: 1261582-58-4
• Molecular Formula: C₈H₆ClNO₂S
• Molecular Weight: 215.66
• Mol file: 1261582-58-4.mol

Synonyms:

Chemical Property of 3-cyano-4-methylbenzene-1-sulfonyl chloride

Chemical Property:

Purity/Quality:

3-cyano-4-methylbenzene-1-sulfonylchloride ^*data from reagent suppliers

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Technology Process of 3-cyano-4-methylbenzene-1-sulfonyl chloride

There total 1 articles about 3-cyano-4-methylbenzene-1-sulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-cyano-4-methylaniline (50670-64-9) → C8H6ClNO2S (1261582-58-4)

Guidance literature:

With tert.-butylnitrite; sulfur dioxide; N-benzyl-N,N,N-triethylammonium chloride; ethylene glycol; copper dichloride; In dichloromethane; acetonitrile; at 0 - 20 ℃; Automated synthesizer;

DOI:10.1039/c0ob00450b

Reference yield:

piperidine (110-89-4) + C8H6ClNO2S (1261582-58-4) → 2-methyl-5-(piperidine-1-sulfonyl)-benzonitrile (1258439-49-4)

Guidance literature:

In dichloromethane; at 20 ℃; for 0.333333h;

DOI:10.1039/c0ob00450b

Reference yield:

C8H6ClNO2S (1261582-58-4) + (R)-1-(4-cyclopropoxybenzyl)pyrrolidin-3-amine hydrochloride → C22H25N3O3S

Guidance literature:

With potassium carbonate; In dichloromethane; water; Inert atmosphere;

DOI:10.1039/c7md00012j

upstream raw materials:

3-cyano-4-methylaniline

Downstream raw materials:

2-methyl-5-(piperidine-1-sulfonyl)-benzonitrile

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