C₁₉H₁₇Cl₂N₃O₃

Base Information

Chemical Name:C₁₉H₁₇Cl₂N₃O₃
CAS No.:120428-77-5
Molecular Formula:C₁₉H₁₇Cl₂N₃O₃
Molecular Weight:406.268
Hs Code.:

C<sub>19</sub>H<sub>17</sub>Cl<sub>2</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₁₇Cl₂N₃O₃

Chemical Property:

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Technology Process of C₁₉H₁₇Cl₂N₃O₃

There total 6 articles about C₁₉H₁₇Cl₂N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67272-12-2
2,2-ethylenedioxy-2,3,4,7-tetrahydroindene

: 120428-77-5
C₁₉H₁₇Cl₂N₃O₃

Guidance literature:: Multi-step reaction with 7 steps

1: MeOH / light petroleum / 6 h / Ambient temperature

2: 92 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

3: 50 percent / lithium diisopropylamide (LDA) / tetrahydrofuran / 2.5 h / 0 - 5 °C

4: 60 percent / Zn/Ag / diethyl ether / 17 h / Heating

5: 60 percent / triethylamine / CH₂Cl₂ / 1 h / 0 - 5 °C

6: 1.) NaBH₄, 2.) 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 1.) methanol, RT, 1 h, 2.) benzene, reflux, 5.5 h

7: 90 percent / CH₂Cl₂ / Ambient temperature

With methanol; sodium tetrahydroborate; silver; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 3-chloro-benzenecarboperoxoic acid; zinc; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; Petroleum ether;

Reference yield:

: 7068-05-5
(3aα,7aα)-8,8-dichloro-2,2-ethylenedioxy-2,3,4,7-tetrahydro-3a,7a-methano-1H-indene

: 120428-77-5
C₁₉H₁₇Cl₂N₃O₃

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / Ambient temperature

2: 50 percent / lithium diisopropylamide (LDA) / tetrahydrofuran / 2.5 h / 0 - 5 °C

3: 60 percent / Zn/Ag / diethyl ether / 17 h / Heating

4: 60 percent / triethylamine / CH₂Cl₂ / 1 h / 0 - 5 °C

5: 1.) NaBH₄, 2.) 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 1.) methanol, RT, 1 h, 2.) benzene, reflux, 5.5 h

6: 90 percent / CH₂Cl₂ / Ambient temperature

With sodium tetrahydroborate; silver; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 3-chloro-benzenecarboperoxoic acid; zinc; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 120428-66-2
(3aα,5β,7aα)-8,8-dichloro-2,2-ethylenedioxy-2,3,4,5-tetrahydro-3a,7a-methano-1H-inden-5-ol

: 120428-77-5
C₁₉H₁₇Cl₂N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / Zn/Ag / diethyl ether / 17 h / Heating

2: 60 percent / triethylamine / CH₂Cl₂ / 1 h / 0 - 5 °C

3: 1.) NaBH₄, 2.) 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 1.) methanol, RT, 1 h, 2.) benzene, reflux, 5.5 h

4: 90 percent / CH₂Cl₂ / Ambient temperature

With sodium tetrahydroborate; silver; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; zinc; In diethyl ether; dichloromethane;