thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside
CAS No.:106927-43-9
Molecular Formula:C₂₈H₄₀N₂O₁₆S₂
Molecular Weight:724.761
Hs Code.:

thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

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Chemical Property of thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

There total 1 articles about thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3068-34-6,38874-23-6,41355-44-6,51236-40-9,74081-14-4,79897-03-3,100759-09-9,109581-83-1
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl chloride

: 1666-13-3
diphenyl diselenide

: 106927-43-9,76235-26-2
thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

: 678968-48-4
phenyl-3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-1-selenenylsulfide-β-d-glucopyranoside

Guidance literature:: 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranosyl chloride; With thiourea; In acetone; for 3h; Reflux;

diphenyl diselenide; With triethylamine; In acetone; at 20 ℃; for 0.75h;
DOI:10.1002/ejoc.201200299

Reference yield: 65.0%

: 106927-43-9,76235-26-2
thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

: 471-35-2
tetramethyldiarsine

: 76235-27-3
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-S-dimethylarsino-1-thio-β-D-glucopyranose

Guidance literature:: In chloroform; for 72h; Ambient temperature;

Reference yield:

: 106927-43-9,76235-26-2
thio [2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose]-(1,1)-S-2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranoside

: 2-acetamido-3,4,6-tri-O-acetyl-1-S-benzoyl-2-deoxy-1-thio-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: tributylphosphine; HCl / dioxane; H₂O / 40 °C

2: pyridine / 16 h / 20 °C

With pyridine; hydrogenchloride; tributylphosphine; In 1,4-dioxane; water; 1: Reduction / 2: Acylation;
DOI:10.1080/07328309908544045