3-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-6-oxo-5-p-chlorophenyl-7-carboethoxymethyl-8-methyl-5H-thiazolo[3,2-a]pyrimido[4,5-d]pyrimidine

Base Information

Chemical Name:3-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-6-oxo-5-p-chlorophenyl-7-carboethoxymethyl-8-methyl-5H-thiazolo[3,2-a]pyrimido[4,5-d]pyrimidine
CAS No.:1338323-98-0
Molecular Formula:C₂₉H₂₅ClN₆O₄S
Molecular Weight:589.074
Hs Code.:

3-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-6-oxo-5-p-chlorophenyl-7-carboethoxymethyl-8-methyl-5H-thiazolo[3,2-a]pyrimido[4,5-d]pyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-6-oxo-5-p-chlorophenyl-7-carboethoxymethyl-8-methyl-5H-thiazolo[3,2-a]pyrimido[4,5-d]pyrimidine

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Technology Process of 3-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-6-oxo-5-p-chlorophenyl-7-carboethoxymethyl-8-methyl-5H-thiazolo[3,2-a]pyrimido[4,5-d]pyrimidine

There total 2 articles about 3-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-6-oxo-5-p-chlorophenyl-7-carboethoxymethyl-8-methyl-5H-thiazolo[3,2-a]pyrimido[4,5-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338323-73-1
C₂₅H₂₄ClN₅O₃S

: 1338323-98-0
3-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-6-oxo-5-p-chlorophenyl-7-carboethoxymethyl-8-methyl-5H-thiazolo[3,2-a]pyrimido[4,5-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol / 1 h / Reflux

1.2: 3 h / Reflux

2.1: sodium acetate / acetic acid / 1 h / Reflux

2.2: 3 h / Reflux

With sodium acetate; sodium hydroxide; In ethanol; acetic acid;
DOI:10.1002/cjoc.201180268

Reference yield:

: 1338323-76-4
2-methyl-7-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-5-p-chlorophenylthiazolo[3,2-a]pyrimido[4,5-d]oxazin-4(5H)-one

: 623-33-6
glycine ethyl ester hydrochloride

: 1338323-98-0
3-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-6-oxo-5-p-chlorophenyl-7-carboethoxymethyl-8-methyl-5H-thiazolo[3,2-a]pyrimido[4,5-d]pyrimidine

Guidance literature:: glycine ethyl ester hydrochloride; With sodium acetate; In acetic acid; for 1h; Reflux;

2-methyl-7-(3-methyl-5-oxo-1-phenyl-2-pyrazolin-4-yl)-5-p-chlorophenylthiazolo[3,2-a]pyrimido[4,5-d]oxazin-4(5H)-one; In acetic acid; for 3h; Reflux;
DOI:10.1002/cjoc.201180268