C₁₃H₁₄N₄O₂S

Base Information

Chemical Name:C₁₃H₁₄N₄O₂S
CAS No.:1334632-43-7
Molecular Formula:C₁₃H₁₄N₄O₂S
Molecular Weight:290.346
Hs Code.:

C<sub>13</sub>H<sub>14</sub>N<sub>4</sub>O<sub>2</sub>S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₄N₄O₂S

Chemical Property:

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Technology Process of C₁₃H₁₄N₄O₂S

There total 4 articles about C₁₃H₁₄N₄O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₄N₄S

: 1334632-43-7
C₁₃H₁₄N₄O₂S

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; at 0 - 20 ℃; for 13h; Inert atmosphere;
DOI:10.1002/chem.201002898

Reference yield:

: 6214-31-9
3-bromo-3-methylbut-1-yne

: 1334632-43-7
C₁₃H₁₄N₄O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: aluminium; mercury dichloride / Inert atmosphere

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere

3: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 13 h / 0 - 20 °C / Inert atmosphere

With hexaammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; aluminium; mercury dichloride; In tetrahydrofuran; ethanol;
DOI:10.1002/chem.201002898

Reference yield:

: 65108-31-8
2,2-dimethyl-but-3-yn-1-ol

: 1334632-43-7
C₁₃H₁₄N₄O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere

2: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 13 h / 0 - 20 °C / Inert atmosphere

With hexaammonium heptamolybdate tetrahydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; In tetrahydrofuran; ethanol;
DOI:10.1002/chem.201002898