C₅₀H₇₈INO₈Si₂

Base Information

Chemical Name:C₅₀H₇₈INO₈Si₂
CAS No.:1378889-88-3
Molecular Formula:C₅₀H₇₈INO₈Si₂
Molecular Weight:1004.25
Hs Code.:

C<sub>50</sub>H<sub>78</sub>INO<sub>8</sub>Si<sub>2</sub>

Synonyms:

Suppliers and Price of C₅₀H₇₈INO₈Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₀H₇₈INO₈Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₀H₇₈INO₈Si₂

There total 2 articles about C₅₀H₇₈INO₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₂₃NO₄

: 1378889-88-3
C₅₀H₇₈INO₈Si₂

: 1378890-09-5
C₅₀H₇₈INO₈Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4.2: 12 h / 20 °C / Inert atmosphere

With hydrogenchloride; zirconocene dichloride; sodium hydride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; 1,4-dioxane; toluene; mineral oil;
DOI:10.1021/ol301103d

Reference yield:

: 1378889-97-4
C₁₅H₂₅NO₄

: 1378889-88-3
C₅₀H₇₈INO₈Si₂

: 1378890-09-5
C₅₀H₇₈INO₈Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: zirconocene dichloride; diisobutylaluminium hydride / tetrahydrofuran; toluene / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 0.5 h / -78 °C / Inert atmosphere

2.1: hydrogenchloride / 1,4-dioxane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

3.2: 12 h / 20 °C / Inert atmosphere

With hydrogenchloride; zirconocene dichloride; diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; 1,4-dioxane; toluene;
DOI:10.1021/ol301103d

Reference yield:

: 1378889-88-3
C₅₀H₇₈INO₈Si₂

: C₆₆H₁₁₁NO₁₂Si₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydrogencarbonate; Dess-Martin periodane; tert-butyl alcohol / dichloromethane / 0.75 h / Inert atmosphere

2.1: 2,6-di-tert-butyl-4-methylpyridine; 1,2-dibromo-1,1,2,2-tetrachloroethane; triphenylphosphine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran; N,N-dimethyl-formamide / 6.08 h / 0 - 20 °C / Inert atmosphere

4.1: barium hydroxide octahydrate / tetrahydrofuran; water / 0.5 h / 20 °C / Inert atmosphere

4.2: 6 h / 20 °C / Inert atmosphere

5.1: (triphenylphosphine)copper(I) hydride hexamer / benzene / 6 h / 20 °C / Inert atmosphere

6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 4 h / 20 °C / pH 7 / Inert atmosphere; aq. buffer

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate / tetrahydrofuran; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-4-methylpyridine; copper(I) thiophene-2-carboxylate; (triphenylphosphine)copper(I) hydride hexamer; barium hydroxide octahydrate; 1,2-dibromo-1,1,2,2-tetrachloroethane; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tert-butyl alcohol; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; benzene; 1.1: Dess-Martin oxidation / 4.1: Horner-Wadsworth-Emmons olefination / 4.2: Horner-Wadsworth-Emmons olefination / 7.1: Stille coupling;
DOI:10.1021/ol301103d