(CO)2Fe(P(C₆H₅)2CH₃)2Br₂

Base Information

Chemical Name:(CO)2Fe(P(C₆H₅)2CH₃)2Br₂
CAS No.:51684-15-2
Molecular Formula:C₂₈H₂₆Br₂FeO₂P₂
Molecular Weight:672.116
Hs Code.:

(CO)2Fe(P(C<sub>6</sub>H<sub>5</sub>)2CH<sub>3</sub>)2Br<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CO)2Fe(P(C₆H₅)2CH₃)2Br₂

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Technology Process of (CO)2Fe(P(C₆H₅)2CH₃)2Br₂

There total 1 articles about (CO)2Fe(P(C₆H₅)2CH₃)2Br₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 18475-84-8
iron(II) carbonyl dibromide

: 1486-28-8
diphenyl(methyl)phosphine

: 51684-15-2
iron(II)(carbonyl)2((phenyl)2methylphosphine)2Br₂

Guidance literature:: In benzene; Dissolving of Fe(CO)4Br2 and PMePh2 under N2 in benzene, mixing of solns. at room temp.. React. is complete in 1 h.; Drying of soln., crystn. of solid residue (n-hexane-CH2Cl2), elem. anal.;

Reference yield: 50.0%

: 51684-15-2,108267-29-4
(CO)2Fe(P(C₆H₅)2CH₃)2Br₂

: 108188-47-2
Fe(CO)(P(CH₃)(C₆H₅)2)2(OCCH₃)I

Guidance literature:: With methyl iodide; In acetonitrile; addn. of alkyl halide at -10°C to a soln. of the complex prepared from dibromo-complex by reduction with Na/Hg in CH3CN at -20°C;

Reference yield: 40.0%

: 51684-15-2
iron(II)(carbonyl)2((phenyl)2methylphosphine)2Br₂

: 108188-47-2
{iron(carbonyl)((phenyl)2methylphosphine)2(η2-CO(methyl))I}*2CH2Cl2

Guidance literature:: With CH₃CN; Na#Hg; CH₃I; In acetonitrile; Dissolving under N2, cooling (-20°C), only partial soln., addn. of sodium amalgam, vigorous stirring (3 h), filtering, keeping at -10°C, equilibrium between Fe3(CO)6(PMePh2)6 and Fe(CO)2(PMePH2)2(MeCN), addn. of CH3I, stirring (5 h).; Drying, crystn. (CH2Cl2) of solid, elem. anal.;