nickel(II) octaethylporphyrin N-oxide

Base Information

Chemical Name:nickel(II) octaethylporphyrin N-oxide
CAS No.:95156-28-8
Molecular Formula:C₃₆H₄₄N₄NiO
Molecular Weight:607.462
Hs Code.:

Synonyms:

Suppliers and Price of nickel(II) octaethylporphyrin N-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of nickel(II) octaethylporphyrin N-oxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of nickel(II) octaethylporphyrin N-oxide

There total 1 articles about nickel(II) octaethylporphyrin N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 67514-01-6
octaethylporphyrine-N-oxide

: 373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6
nickel diacetate

: 24803-99-4
nickel(II) octaethylporphyrin

: 95156-28-8
nickel(II) octaethylporphyrin N-oxide

Guidance literature:: With ammonia; In methanol; dichloromethane; addn. of MeOH satd. with NH3 and nickel acetate to a soln. of octaethylporphyrin N-oxide in CH2Cl2, refluxing under Ar for 24 h; cooling, evapn. in vac., dissolving in CH2Cl2, washing (aq. NH3, H2O), concg. in vac., column chromy. (silica gel, hexane/CH2Cl2) gives a pink fraction of Ni-octaethylporphyrin, elution with CH2Cl2, evapn. in vac., recrystn. (CH2Cl2/MeOH), elem. anal.;
DOI:10.1021/ja00294a033

Reference yield:

: 95156-28-8
nickel(II) octaethylporphyrin N-oxide

: 24803-99-4
octaethylphorphyrinato nickel

: 100762-96-7
nickel(II) octaethyloxochlorin

Guidance literature:: In xylene; refluxing Ni(II) octaethylporphyrin N-oxide in xylene under Ar for 30 min; evapn., chromy. (silica gel, hexane/benzene (1:1)): first band containsNi(II) octaethylporphyrin, second band contains Ni(II) octaethyloxochlorin, third band not identified (5:2:3 ratio);
DOI:10.1016/S0020-1693(00)84399-6