methyl 3-chloro-2-<(benzyloxycarbonyl)amino>-1-propanesulfonate

Base Information

• Chemical Name: methyl 3-chloro-2-<(benzyloxycarbonyl)amino>-1-propanesulfonate
• CAS No.: 79409-92-0
• Molecular Formula: C₁₂H₁₆ClNO₅S
• Molecular Weight: 321.782

Synonyms:

Chemical Property of methyl 3-chloro-2-<(benzyloxycarbonyl)amino>-1-propanesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of methyl 3-chloro-2-<(benzyloxycarbonyl)amino>-1-propanesulfonate

There total 2 articles about methyl 3-chloro-2-<(benzyloxycarbonyl)amino>-1-propanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((R)-1-Hydroxymethyl-2-mercapto-ethyl)-carbamic acid benzyl ester → methyl 3-chloro-2-<(benzyloxycarbonyl)amino>-1-propanesulfonate (79409-92-0)

Guidance literature:

Multi-step reaction with 3 steps

1: iodine, pyridine / methanol

2: 78 percent / chlorine / acetic acid; CH₂Cl₂ / 2 h / Ambient temperature

3: 43 percent / CH₂Cl₂

With pyridine; iodine; chlorine; In methanol; dichloromethane; acetic acid;

DOI:10.1021/jo00339a034

Reference yield:

Z-L-cystinol (79409-89-5) → methyl 3-chloro-2-<(benzyloxycarbonyl)amino>-1-propanesulfonate (79409-92-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / chlorine / acetic acid; CH₂Cl₂ / 2 h / Ambient temperature

2: 43 percent / CH₂Cl₂

With chlorine; In dichloromethane; acetic acid;

DOI:10.1021/jo00339a034

upstream raw materials:

Z-L-cystinol

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