[(((((CH₃)3C)C₆H₂CH₂NH(CH₂CH₂NH)2CH₂)2(SCH₂CH₂S))Ni₂Cl₂)2(Cl)3]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[((C₃₄H₅₆N₆S₂)Ni₂Cl₂)2(Cl)3]B(C₆H₅)4

Base Information

• Chemical Name: [(((((CH₃)3C)C₆H₂CH₂NH(CH₂CH₂NH)2CH₂)2(SCH₂CH₂S))Ni₂Cl₂)2(Cl)3]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[((C₃₄H₅₆N₆S₂)Ni₂Cl₂)2(Cl)3]B(C₆H₅)4
• CAS No.: 382655-02-9
• Molecular Formula: C₂₄H₂₀B*C₆₈H₁₁₂Cl₇N₁₂Ni₄S₄
• Molecular Weight: 2028.15
• Mol file: 382655-02-9.mol

Synonyms:

Chemical Property of [(((((CH₃)3C)C₆H₂CH₂NH(CH₂CH₂NH)2CH₂)2(SCH₂CH₂S))Ni₂Cl₂)2(Cl)3]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[((C₃₄H₅₆N₆S₂)Ni₂Cl₂)2(Cl)3]B(C₆H₅)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(((((CH₃)3C)C₆H₂CH₂NH(CH₂CH₂NH)2CH₂)2(SCH₂CH₂S))Ni₂Cl₂)2(Cl)3]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[((C₃₄H₅₆N₆S₂)Ni₂Cl₂)2(Cl)3]B(C₆H₅)4

There total 1 articles about [(((((CH₃)3C)C₆H₂CH₂NH(CH₂CH₂NH)2CH₂)2(SCH₂CH₂S))Ni₂Cl₂)2(Cl)3]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[((C₃₄H₅₆N₆S₂)Ni₂Cl₂)2(Cl)3]B(C₆H₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

[(((((CH3)3C)C6H2CH2NHCH2CH2NHCH2CH2NHCH2)2(SCH2CH2S))Ni2Cl2)2(Cl)3](1+)*Cl(1-)=[((C34H56N6S2)Ni2Cl2)2(Cl)3]Cl (381225-58-7) + sodium tetraphenyl borate (143-66-8) → [(((((CH3)3C)C6H2CH2NH(CH2CH2NH)2CH2)2(SCH2CH2S))Ni2Cl2)2(Cl)3](1+)*B(C6H5)4(1-)=[((C34H56N6S2)Ni2Cl2)2(Cl)3]B(C6H5)4 (382655-02-9)

Guidance literature:

In acetonitrile; all manipulations under Ar atm.; to soln. of complex added solid B compd.; volume of solvent reduced in vac., filtered, washed with MeCN and Et2O, dried in vac., elem. anal.;

DOI:10.1515/znb-2001-0907

upstream raw materials:

[(((((CH₃)3C)C₆H₂CH₂NHCH₂CH₂NHCH₂CH₂NHCH₂)2(SCH₂CH₂S))Ni₂Cl₂)2(Cl)3]⁽¹⁺⁾*Cl^(1-)=[((C₃₄H₅₆N₆S₂)Ni₂Cl₂)2(Cl)3]Cl

sodium tetraphenyl borate