(+/-)-phthalic acid mono-(5exo,6exo-bis-methoxycarbonyl-[2exo]norbornyl ester)

Base Information

Chemical Name:(+/-)-phthalic acid mono-(5exo,6exo-bis-methoxycarbonyl-[2exo]norbornyl ester)
CAS No.:111357-76-7
Molecular Formula:C₁₉H₂₀O₈
Molecular Weight:376.363
Hs Code.:

(+/-)-phthalic acid mono-(5<i>exo</i>,6<i>exo</i>-bis-methoxycarbonyl-[2<i>exo</i>]norbornyl ester)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-phthalic acid mono-(5exo,6exo-bis-methoxycarbonyl-[2exo]norbornyl ester)

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Technology Process of (+/-)-phthalic acid mono-(5exo,6exo-bis-methoxycarbonyl-[2exo]norbornyl ester)

There total 3 articles about (+/-)-phthalic acid mono-(5exo,6exo-bis-methoxycarbonyl-[2exo]norbornyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6004-80-4,119238-43-6
5exo,6exo-epoxy-norbornane-2exo,3exo-dicarboxylic acid-anhydride

: 111357-76-7
(+/-)-phthalic acid mono-(5exo,6exo-bis-methoxycarbonyl-[2exo]norbornyl ester)

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃; HBr; acetic acid / Erwaermen des Reaktionsprodukts mit Raney-Nickel in H₂O

2: diethyl ether / Erwaermen des Reaktionsprodukts mit Phthalsaeure-anhydrid und Pyridin

With diethyl ether; chloroform; hydrogen bromide; acetic acid;
DOI:10.1021/ja01549a058

Reference yield:

: 2746-19-2
(1R,2R,6S,7S)-4-oxa-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

: 111357-76-7
(+/-)-phthalic acid mono-(5exo,6exo-bis-methoxycarbonyl-[2exo]norbornyl ester)

Guidance literature:: Multi-step reaction with 3 steps

2: CHCl₃; HBr; acetic acid / Erwaermen des Reaktionsprodukts mit Raney-Nickel in H₂O

3: diethyl ether / Erwaermen des Reaktionsprodukts mit Phthalsaeure-anhydrid und Pyridin

With diethyl ether; chloroform; hydrogen bromide; acetic acid;
DOI:10.1021/ja01549a058