[Mn₂Ce₃O₆(p-toluic acid)6(NO₃)2(dmf)4]*H₂O

Base Information

Chemical Name:[Mn₂Ce₃O₆(p-toluic acid)6(NO₃)2(dmf)4]*H₂O
CAS No.:1353054-78-0
Molecular Formula:C₆₀H₇₀Ce₃Mn₂N₆O₂₈*H₂O
Molecular Weight:1871.49
Hs Code.:

[Mn<sub>2</sub>Ce<sub>3</sub>O<sub>6</sub>(p-toluic acid)6(NO<sub>3</sub>)2(dmf)4]*H<sub>2</sub>O

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Chemical Property of [Mn₂Ce₃O₆(p-toluic acid)6(NO₃)2(dmf)4]*H₂O

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Technology Process of [Mn₂Ce₃O₆(p-toluic acid)6(NO₃)2(dmf)4]*H₂O

There total 2 articles about [Mn₂Ce₃O₆(p-toluic acid)6(NO₃)2(dmf)4]*H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: cerium(IV) ammonium nitrate

: Mn(p-toluic acid)2*2H₂O

: 80937-33-3
oxygen

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: [Mn₈CeO₈(p-toluic acid)12(dmf)4]

: 1353054-78-0
[Mn₂Ce₃O₆(p-toluic acid)6(NO₃)2(dmf)4]*H₂O

Guidance literature:: With 4,4'-bipyridine; In ethanol; N,N-dimethyl-formamide; aerobic conditions; 4,4'-bipy added to stirred soln. of Mn(pta)2 in EtOH/dmf, then solid Ce nitrate added over 0.5 h, then stirring overnight atroom temp. produces dark soln. with suspended brown material; Mn2Ce3O6(p-toluic acid)6(NO3)2(dmf)4*H2O isolated from soln. while brownresidue dissolved in dmf/dmso/CHCl3, soln. evapd. naturally (1 wk.), cr ystals filtered, dried (air); elem. anal., XRD;
DOI:10.1002/ejic.201100719

Reference yield: 22.0%

: cerium(IV) ammonium nitrate

: Mn(p-toluic acid)2*2H₂O

: 80937-33-3
oxygen

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1353054-78-0
[Mn₂Ce₃O₆(p-toluic acid)6(NO₃)2(dmf)4]*H₂O

Guidance literature:: In ethanol; N,N-dimethyl-formamide; aerobic conditions; then solid Ce nitrate over 1 h added to Mn(pta)2 in EtOH/dmf soln., stirring at room temp. for 4 h; filtered, kept several wk. at room temp., crystals filtered, washed (H2O), dried (air), recrystn. (MeCN); elem. anal., XRD;
DOI:10.1002/ejic.201100719