acide benzodioxine (1,3)> carboxylique-2 cis

Base Information

Chemical Name:acide benzodioxine (1,3)> carboxylique-2 cis
CAS No.:67059-70-5
Molecular Formula:C₁₆H₁₄O₄
Molecular Weight:270.285
Hs Code.:

acide <methyl-4 phenyl-4 <4H> benzodioxine (1,3)> carboxylique-2 cis

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Chemical Property of acide benzodioxine (1,3)> carboxylique-2 cis

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Technology Process of acide benzodioxine (1,3)> carboxylique-2 cis

There total 7 articles about acide benzodioxine (1,3)> carboxylique-2 cis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 67059-69-2,67059-71-6,86616-95-7,86616-96-8
benzodioxine (1,3)> carboxylate-2 de methyle cis

: 67059-70-5,67059-72-7,86616-93-5,86616-94-6
acide benzodioxine (1,3)> carboxylique-2 cis

Guidance literature:: With potassium hydroxide; In methanol; water; for 16h; Ambient temperature;

Reference yield: 55.0%

: 67059-69-2,67059-71-6,86616-95-7,86616-96-8
benzodioxine (1,3)> carboxylate-2 de methyle trans

: 67059-70-5,67059-72-7,86616-93-5,86616-94-6
acide benzodioxine (1,3)> carboxylique-2 trans

Guidance literature:: With potassium hydroxide; In methanol; water; for 16h; Ambient temperature;

Reference yield:

: 67059-77-2
acide benzodioxine-(1,3)> caboxylique-2

: 67059-70-5,67059-72-7,86616-93-5,86616-94-6
acide benzodioxine (1,3)> carboxylique-2 trans

Guidance literature:: Multi-step reaction with 3 steps

1: 1 g / CH₂Cl₂ / 24 h

2: 92.2 percent / H₂, Et₃N / 10percent Pd-C / ethanol / Ambient temperature

3: 55 percent / KOH / H₂O; methanol / 16 h / Ambient temperature

With potassium hydroxide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water;