C₁₅H₁₇NO₃

Base Information

Chemical Name:C₁₅H₁₇NO₃
CAS No.:1360562-85-1
Molecular Formula:C₁₅H₁₇NO₃
Molecular Weight:259.305
Hs Code.:

C<sub>15</sub>H<sub>17</sub>NO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₇NO₃

Chemical Property:

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Technology Process of C₁₅H₁₇NO₃

There total 10 articles about C₁₅H₁₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355075-81-8
(5S,2E)-(+)-methyl (3,4-dihydro-5-phenyl-2H-pyrrol-2-yl)-but-2-enoate

: 1360562-85-1
C₁₅H₁₇NO₃

Guidance literature:: With urea hydrogen peroxide adduct; methyltrioxorhenium(VII); In methanol; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/jo202652f

Reference yield:

: 1360562-73-7
(Ss,3S)-(+)-N-(p-toluenesulfinyl)-3-amino-5-(2-phenyl-1,3-dioxolan-2-yl)pentanal

: 1360562-85-1
C₁₅H₁₇NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: hydrogenchloride / tetrahydrofuran; methanol; water / 16 h / 20 °C

3.1: urea hydrogen peroxide adduct; methyltrioxorhenium(VII) / methanol / 15 h / 20 °C / Inert atmosphere

With hydrogenchloride; urea hydrogen peroxide adduct; methyltrioxorhenium(VII); 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1021/jo202652f

Reference yield:

: (S)-(+)-3-(2-phenyl-1,3-dioxolan-2-yl)propylidene-p-toluenesulfinamide

: 1360562-85-1
C₁₅H₁₇NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 1 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: hydrogenchloride / tetrahydrofuran; methanol; water / 16 h / 20 °C

5.1: urea hydrogen peroxide adduct; methyltrioxorhenium(VII) / methanol / 15 h / 20 °C / Inert atmosphere

With hydrogenchloride; sodium hexamethyldisilazane; urea hydrogen peroxide adduct; methyltrioxorhenium(VII); diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; diethyl ether; water; toluene; acetonitrile;
DOI:10.1021/jo202652f