[(tert-butyl isocyanide)tris(η(5)-cyclopentadienyl)zirconium] methyltris(pentafluorophenyl)borate

Base Information

• Chemical Name: [(tert-butyl isocyanide)tris(η(5)-cyclopentadienyl)zirconium] methyltris(pentafluorophenyl)borate
• CAS No.: 185549-34-2
• Molecular Formula: C₁₉H₃BF₁₅*C₂₀H₂₄NZr
• Molecular Weight: 896.661
• Mol file: 185549-34-2.mol

Synonyms:

Chemical Property of [(tert-butyl isocyanide)tris(η(5)-cyclopentadienyl)zirconium] methyltris(pentafluorophenyl)borate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(tert-butyl isocyanide)tris(η(5)-cyclopentadienyl)zirconium] methyltris(pentafluorophenyl)borate

There total 1 articles about [(tert-butyl isocyanide)tris(η(5)-cyclopentadienyl)zirconium] methyltris(pentafluorophenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

tris(η(5)-cyclopentadienyl)methylzirconium + tert-butylisonitrile (119072-55-8,7188-38-7) + tris(pentafluorophenyl)borate (1109-15-5) → [(tert-butyl isocyanide)tris(η(5)-cyclopentadienyl)zirconium] methyltris(pentafluorophenyl)borate (185549-34-2)

Guidance literature:

In dichloromethane; Ar-atmosphere; addn. of cold CH2Cl2 (-78°C) to cold (-78°C) B-compd. and Zr-compd., slight warming, recooling to -78°C, t-BuNC addn. (excess), warming to room temp.; concg., pptn. on pentane addn., filtration, washing (pentane), drying (vac.); elem. anal.;

DOI:10.1021/om960777u

upstream raw materials:

tert-butylisonitrile

tris(pentafluorophenyl)borate