4β,8β-Epoxy-4,5,8,8a-tetrahydro-(3a-αH,8a-αH)-3aH-cycloheptaisoxazol-6(7H)-on

Base Information

• Chemical Name: 4β,8β-Epoxy-4,5,8,8a-tetrahydro-(3a-αH,8a-αH)-3aH-cycloheptaisoxazol-6(7H)-on
• CAS No.: 139781-12-7
• Molecular Formula: C₁₄H₁₃NO₃
• Molecular Weight: 243.262
• Mol file: 139781-12-7.mol

Synonyms:

Chemical Property of 4β,8β-Epoxy-4,5,8,8a-tetrahydro-(3a-αH,8a-αH)-3aH-cycloheptaisoxazol-6(7H)-on

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4β,8β-Epoxy-4,5,8,8a-tetrahydro-(3a-αH,8a-αH)-3aH-cycloheptaisoxazol-6(7H)-on

There total 1 articles about 4β,8β-Epoxy-4,5,8,8a-tetrahydro-(3a-αH,8a-αH)-3aH-cycloheptaisoxazol-6(7H)-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

8-oxabicyclo[3.2.1]oct-6-en-3-one (40458-77-3) + benzohydroximoyl chloride (698-16-8) → 4β,8β-Epoxy-4,5,8,8a-tetrahydro-(3a-αH,8a-αH)-3aH-cycloheptaisoxazol-6(7H)-on (139781-12-7)

Guidance literature:

With triethylamine; In tetrahydrofuran; Ambient temperature;

DOI:10.1002/ardp.19923250205

upstream raw materials:

8-oxabicyclo[3.2.1]oct-6-en-3-one

benzohydroximoyl chloride