bis(tetramethylammonium) ostakis(benzenethiolato)hexaargentate(I)

Base Information

Chemical Name:bis(tetramethylammonium) ostakis(benzenethiolato)hexaargentate(I)
CAS No.:76402-94-3
Molecular Formula:6Ag*2C₄H₁₂N*8C₆H₅S
Molecular Weight:1668.87
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(tetramethylammonium) ostakis(benzenethiolato)hexaargentate(I)

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Technology Process of bis(tetramethylammonium) ostakis(benzenethiolato)hexaargentate(I)

There total 1 articles about bis(tetramethylammonium) ostakis(benzenethiolato)hexaargentate(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-57-0
tetramethlyammonium chloride

: 108-98-5
thiophenol

: 76402-94-3
bis(tetramethylammonium) ostakis(benzenethiolato)hexaargentate(I)

Guidance literature:: With tri-n-butylamine; AgNO₃; In methanol; acetonitrile; to a soln. of C6H5SH and N(C4H9)3 in MeCN was added a soln. of Me4NCl in MeOH, followed by a soln. of AgNO3 in MeCN at 20°C; abs. EtOH was added and mixt. was sealed and stored at 0°C for 6days, ppt. was washed with EtOH, dried in vac.; elem.anal.;
DOI:10.1021/ic50219a031

Reference yield:

: 76402-94-3
bis(tetramethylammonium) ostakis(benzenethiolato)hexaargentate(I)

: 22758-12-9
silver(I) benzenethiolate

Guidance literature:: In acetonitrile; byproducts: PhS(1-); complex was dissolved in MeCN, product ppt. slowly at room temp. and rapidly on heating;
DOI:10.1021/ic50219a031