octacarbonyl-1κ2C,2κ3C,3κ3C-cyclopentadienyl-1(η5)-[μ3-dimethyl(phenylethynyl-2κ2C,C':3κ2C,C')silyl-1κSi]-1-iron(II)-2,3-bis[cobalt(0)][Co-Co]

Base Information

• Chemical Name: octacarbonyl-1κ2C,2κ3C,3κ3C-cyclopentadienyl-1(η5)-[μ3-dimethyl(phenylethynyl-2κ2C,C':3κ2C,C')silyl-1κSi]-1-iron(II)-2,3-bis[cobalt(0)][Co-Co]
• CAS No.: 1367364-03-1
• Molecular Formula: C₂₃H₁₆Co₂FeO₈Si
• Molecular Weight: 622.294
• Mol file: 1367364-03-1.mol

Synonyms:

Chemical Property of octacarbonyl-1κ2C,2κ3C,3κ3C-cyclopentadienyl-1(η5)-[μ3-dimethyl(phenylethynyl-2κ2C,C':3κ2C,C')silyl-1κSi]-1-iron(II)-2,3-bis[cobalt(0)][Co-Co]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of octacarbonyl-1κ2C,2κ3C,3κ3C-cyclopentadienyl-1(η5)-[μ3-dimethyl(phenylethynyl-2κ2C,C':3κ2C,C')silyl-1κSi]-1-iron(II)-2,3-bis[cobalt(0)][Co-Co]

There total 1 articles about octacarbonyl-1κ2C,2κ3C,3κ3C-cyclopentadienyl-1(η5)-[μ3-dimethyl(phenylethynyl-2κ2C,C':3κ2C,C')silyl-1κSi]-1-iron(II)-2,3-bis[cobalt(0)][Co-Co] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

dicobalt octacarbonyl (15226-74-1,61091-28-9,61117-58-6) + dicarbonyl(η5-cyclopentadienyl)dimethyl(phenylethynyl)silyliron(II) (1367364-00-8) → octacarbonyl-1κ2C,2κ3C,3κ3C-cyclopentadienyl-1(η5)-[μ3-dimethyl(phenylethynyl-2κ2C,C':3κ2C,C')silyl-1κSi]-1-iron(II)-2,3-bis[cobalt(0)][Co-Co] (1367364-03-1)

Guidance literature:

In hexane; byproducts: CO; Ar, stirred for 1 d; filtered, slowly concd. (vac.), cooled (-20°C), ppt. dried (vac.), recrystd. (hexane); elem. anal.;

DOI:10.1016/j.jorganchem.2012.01.019

upstream raw materials:

dicobalt octacarbonyl

dicarbonyl(η5-cyclopentadienyl)dimethyl(phenylethynyl)silyliron(II)