meso-2,3-dihydroxy-2,3-dimethyl-succinic acid

Base Information

• Chemical Name: meso-2,3-dihydroxy-2,3-dimethyl-succinic acid
• CAS No.: 14812-52-3
• Molecular Formula: C₆H₁₀O₆
• Molecular Weight: 178.142
• Mol file: 14812-52-3.mol

Synonyms:

Chemical Property of meso-2,3-dihydroxy-2,3-dimethyl-succinic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of meso-2,3-dihydroxy-2,3-dimethyl-succinic acid

There total 1 articles about meso-2,3-dihydroxy-2,3-dimethyl-succinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-oxo-propionic acid (127-17-3) → LACTIC ACID (849585-22-4,106989-11-1,26811-96-1,31587-11-8,26100-51-6) + meso-2,3-dihydroxy-2,3-dimethyl-succinic acid (14812-52-3)

Guidance literature:

With ammonium pyruvate; water; Electrolysis_.in einer Loesung vom pH 2-5 an einer Quecksilber-Kupfer-Kathode;

DOI:10.1021/jo01101a018

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + meso-2,3-dihydroxy-2,3-dimethyl-succinic acid (14812-52-3) → meso-dimethyl 2,3-dimethyltartrate (15309-47-4)

Guidance literature:

With diethyl ether;

DOI:10.1021/jo01101a018

Reference yield:

antimony(III) trioxide + (+/-)-dimethyltartaric acid (6863-95-2,14812-52-3,14812-53-4,34618-92-3,54809-00-6,74543-88-7) → 2Na(1+)*Sb2(C6H6O6)2(2-)*4H2O = Na2[Sb2(C6H6O6)2]*4H2O

Guidance literature:

With NaOH; In water; a slurry of Sb2O3, NaOH and (+/-)-dimethyltartaric acid in molar ratio of 1:2.2 heated for several days; filtered; pptd. by addn. of 95% ethanol to the warmed soln.; collected;washed with aqueous ethanol and acetone; air dried; elem. anal.;

DOI:10.1021/ja00538a002

upstream raw materials:

2-oxo-propionic acid

Downstream raw materials:

meso-dimethyl 2,3-dimethyltartrate