C₃₃H₃₈N₄O₆S₂*C₂HF₃O₂

Base Information

Chemical Name:C₃₃H₃₈N₄O₆S₂*C₂HF₃O₂
CAS No.:1586761-35-4
Molecular Formula:C₂HF₃O₂*C₃₃H₃₈N₄O₆S₂
Molecular Weight:764.844
Hs Code.:

C<sub>33</sub>H<sub>38</sub>N<sub>4</sub>O<sub>6</sub>S<sub>2</sub>*C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>

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Chemical Property of C₃₃H₃₈N₄O₆S₂*C₂HF₃O₂

Chemical Property:

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Technology Process of C₃₃H₃₈N₄O₆S₂*C₂HF₃O₂

There total 10 articles about C₃₃H₃₈N₄O₆S₂*C₂HF₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 925893-46-5
Fmoc-Phe-Lys(Boc)-OtBu

: 1586761-35-4
C₃₃H₃₈N₄O₆S₂*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine / dichloromethane / 3 h / Inert atmosphere

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: dichloromethane / 4 h / Inert atmosphere

With piperidine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1002/chem.201304064

Reference yield:

: 1586761-13-8
methyl 2-(3,4-dibromo-2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)acetate

: 1586761-35-4
C₃₃H₃₈N₄O₆S₂*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; sodium iodide / Reflux

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride / 1,4-dioxane / 3 h / Inert atmosphere; Reflux

3.1: lithium iodide / ethyl acetate / Reflux

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / Inert atmosphere

4.2: 20 °C / Inert atmosphere

5.1: dichloromethane / 4 h / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; cesium fluoride; sodium iodide; lithium iodide; In 1,4-dioxane; dichloromethane; ethyl acetate; 2.1: |Suzuki Coupling;
DOI:10.1002/chem.201304064

Reference yield:

: 638-02-8
2,5-DIMETHYLTHIOPHENE

: 1586761-35-4
C₃₃H₃₈N₄O₆S₂*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: acetic acid; N-Bromosuccinimide / 2 h

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; cesium fluoride / 1,4-dioxane / 3 h / Inert atmosphere; Reflux

4.1: lithium iodide / ethyl acetate / Reflux

5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / Inert atmosphere

5.2: 20 °C / Inert atmosphere

6.1: dichloromethane / 4 h / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; cesium fluoride; lithium iodide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; ethyl acetate; 3.1: |Suzuki Coupling;
DOI:10.1002/chem.201304064