N-1-(3-hydroxyphenyl) (Z)-9-hexadecenamide

Base Information

Chemical Name:N-1-(3-hydroxyphenyl) (Z)-9-hexadecenamide
CAS No.:224455-17-8
Molecular Formula:C₂₂H₃₅NO₂
Molecular Weight:345.525
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-1-(3-hydroxyphenyl) (Z)-9-hexadecenamide

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Technology Process of N-1-(3-hydroxyphenyl) (Z)-9-hexadecenamide

There total 1 articles about N-1-(3-hydroxyphenyl) (Z)-9-hexadecenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 40426-22-0
( Z )-hexadec-9-enoyl chloride

: 591-27-5
m-Hydroxyaniline

: 224455-17-8
N-1-(3-hydroxyphenyl) (Z)-9-hexadecenamide

Guidance literature:: In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jm970809v

Reference yield:

: 224455-17-8
N-1-(3-hydroxyphenyl) (Z)-9-hexadecenamide

: Phosphoric acid mono-[3-((Z)-hexadec-9-enoylamino)-phenyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) tetrazole, 2.) 30 percent aq. H₂O₂ / 1.) THF, CH₂Cl₂, RT, overnight, 2.) THF, CH₂Cl₂, 2 h

2: 100 percent / 10 percent Pd/C / tetrahydrofuran; cyclohexene / 4 h / 78 °C

With 1H-tetrazole; palladium on activated charcoal; dihydrogen peroxide; In tetrahydrofuran; cyclohexene;
DOI:10.1021/jm970809v

Reference yield:

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 224455-17-8
N-1-(3-hydroxyphenyl) (Z)-9-hexadecenamide

: 224455-34-9
dibenzyl (3-((Z)-9-hexadecenoylamino)phenyl) phosphate

Guidance literature:: With 1H-tetrazole; dihydrogen peroxide; Yield given; Multistep reaction; 1.) THF, CH₂Cl₂, RT, overnight, 2.) THF, CH₂Cl₂, 2 h;
DOI:10.1021/jm970809v