-O-methylester-S-anilid

Base Information

• Chemical Name: -O-methylester-S-anilid
• CAS No.: 7113-65-7
• Molecular Formula: C₁₂H₁₅NO₂S
• Molecular Weight: 237.323

Synonyms:

Chemical Property of -O-methylester-S-anilid

Chemical Property:

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Technology Process of -O-methylester-S-anilid

There total 1 articles about -O-methylester-S-anilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4-dimethoxy-3,3-dimethyl-1-phenyl-azetidine-2-thione (7113-62-4) → -O-methylester-S-anilid (7113-65-7)

Guidance literature:

With water; In 1,4-dioxane; for 4h; Heating;

Reference yield:

-O-methylester-S-anilid (7113-65-7) → -S-anilid

Guidance literature:

With sodium hydroxide; at 60 ℃; for 3h;

Reference yield:

-O-methylester-S-anilid (7113-65-7) → methyl-2 N-phenyl propanethioamide (7113-66-8)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NaOH / 3 h / 60 °C

2: 0.25 h / 75 - 80 °C

With sodium hydroxide;

upstream raw materials:

4,4-dimethoxy-3,3-dimethyl-1-phenyl-azetidine-2-thione

Downstream raw materials:

methyl-2 N-phenyl propanethioamide

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