1--2,2,3-tris(carbomethoxy)cyclobutane

Base Information

Chemical Name:1--2,2,3-tris(carbomethoxy)cyclobutane
CAS No.:72541-97-0
Molecular Formula:C₁₈H₂₃NO₆
Molecular Weight:349.384
Hs Code.:

1-<p-(dimethylamino)phenyl>-2,2,3-tris(carbomethoxy)cyclobutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1--2,2,3-tris(carbomethoxy)cyclobutane

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Technology Process of 1--2,2,3-tris(carbomethoxy)cyclobutane

There total 4 articles about 1--2,2,3-tris(carbomethoxy)cyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 51175-48-5
ethene-1,1,2-tricarboxylic acid trimethyl ester

: 2039-80-7
N,N-dimethy-4-vinylaniline

: 72541-97-0
1--2,2,3-tris(carbomethoxy)cyclobutane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In benzene; at 70 ℃; for 16h; Product distribution;
DOI:10.1021/jo01293a015

Reference yield: 30.0%

: 51175-48-5
ethene-1,1,2-tricarboxylic acid trimethyl ester

: 2039-80-7
N,N-dimethy-4-vinylaniline

: 72541-97-0
1--2,2,3-tris(carbomethoxy)cyclobutane

Guidance literature:: In acetonitrile; Heating;
DOI:10.1021/jo01293a015

Reference yield:

: 100-10-7
4-dimethylamino-benzaldehyde

: 72541-97-0
1--2,2,3-tris(carbomethoxy)cyclobutane

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Mg / 1) diethyl ether, 1h; 2) diethyl ether, 3h

2: flash distillation at 150 deg C under vacuum

3: 30 percent / acetonitrile / Heating

With magnesium; In acetonitrile;
DOI:10.1021/jo01293a015