4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-{(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-tetrahydro-pyran-2-yloxy}-tetrahydro-pyran-2-ylmethyl ester

Base Information

• Chemical Name: 4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-{(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-tetrahydro-pyran-2-yloxy}-tetrahydro-pyran-2-ylmethyl ester
• CAS No.: 74501-34-1
• Molecular Formula: C₁₀₆H₁₄₂O₁₅
• Molecular Weight: 1656.28

Synonyms:

Chemical Property of 4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-{(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-tetrahydro-pyran-2-yloxy}-tetrahydro-pyran-2-ylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-{(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-tetrahydro-pyran-2-yloxy}-tetrahydro-pyran-2-ylmethyl ester

There total 2 articles about 4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-{(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-tetrahydro-pyran-2-yloxy}-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Potassium; 4-(4-hexadecyloxy-phenyl)-butyrate (74501-37-4) + 2,3,4,2',3',4'-hexa-O-benzyl-6,6'-di-O-(methylsulfonyl)-α,α-trehalose (74512-35-9) → 4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-{(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-tetrahydro-pyran-2-yloxy}-tetrahydro-pyran-2-ylmethyl ester (74501-34-1)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; at 90 - 95 ℃; for 3h; Yield given;

DOI:10.1016/S0008-6215(00)85692-X

Reference yield:

p-hexadecyloxyphenyl-4-butanoyl chloride (74501-38-5) + [(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl]-methanol (125177-97-1,128188-35-2,74501-33-0) → 4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-{(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-tetrahydro-pyran-2-yloxy}-tetrahydro-pyran-2-ylmethyl ester (74501-34-1)

Guidance literature:

Yield given;

DOI:10.1016/S0008-6215(00)85692-X

Reference yield:

4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-{(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-tetrahydro-pyran-2-yloxy}-tetrahydro-pyran-2-ylmethyl ester (74501-34-1) → 4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3S,4S,5R,6R)-6-{(2R,3R,4S,5S,6R)-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy}-3,4,5-trihydroxy-tetrahydro-pyran-2-ylmethyl ester (74501-35-2)

Guidance literature:

palladium on activated charcoal; for 3h; Yield given;

DOI:10.1016/S0008-6215(00)85692-X

upstream raw materials:

p-hexadecyloxyphenyl-4-butanoyl chloride

[(2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yl]-methanol

Potassium; 4-(4-hexadecyloxy-phenyl)-butyrate

2,3,4,2',3',4'-hexa-O-benzyl-6,6'-di-O-(methylsulfonyl)-α,α-trehalose

Downstream raw materials:

4-(4-Hexadecyloxy-phenyl)-butyric acid (2R,3S,4S,5R,6R)-6-{(2R,3R,4S,5S,6R)-6-[4-(4-hexadecyloxy-phenyl)-butyryloxymethyl]-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy}-3,4,5-trihydroxy-tetrahydro-pyran-2-ylmethyl ester

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