C₃₃H₄₅ClN₄O₇

Base Information

Chemical Name:C₃₃H₄₅ClN₄O₇
CAS No.:245116-23-8
Molecular Formula:C₃₃H₄₅ClN₄O₇
Molecular Weight:645.196
Hs Code.:

C<sub>33</sub>H<sub>45</sub>ClN<sub>4</sub>O<sub>7</sub>

Synonyms:

Suppliers and Price of C₃₃H₄₅ClN₄O₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₄₅ClN₄O₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₄₅ClN₄O₇

There total 10 articles about C₃₃H₄₅ClN₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 591-35-5
3,5-dichlorophenol

: 245116-23-8
C₃₃H₄₅ClN₄O₇

Guidance literature:: Multi-step reaction with 10 steps

1: 100 percent / DMAP; DIEA / CH₂Cl₂

2: 64 percent / Mg / tetrahydrofuran / -78 °C

3: 96 percent / oxalyl chloride; DMF / CH₂Cl₂

4: 91 percent / TBAF / tetrahydrofuran

5: 83 percent / Cs₂CO₃ / acetonitrile / 50 °C

6: 95 percent / Ph₃P; DEAD / tetrahydrofuran

7: 64 percent / aq. MeNH₂ / tetrahydrofuran

8: 85 percent / dimethylformamide

9: 70 percent / aq. NaOH / ethanol

10: benzotriazol-1-yloxytri(dimethylamino)phosphonium*PF₆^(1-); dimethylaminomethyl-polystyrene resin; Et₃N / CH₂Cl₂

With dmap; sodium hydroxide; oxalyl dichloride; dimethylaminomethyl-polystyrene resin; tetrabutyl ammonium fluoride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; magnesium; triethylamine; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; triphenylphosphine; methylamine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 6: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2004.05.002

Reference yield:

: 126663-61-4
1-<(tert-butyldimethylsilyl)oxy>-3,5-dichlorobenzene

: 245116-23-8
C₃₃H₄₅ClN₄O₇

Guidance literature:: Multi-step reaction with 9 steps

1: 64 percent / Mg / tetrahydrofuran / -78 °C

2: 96 percent / oxalyl chloride; DMF / CH₂Cl₂

3: 91 percent / TBAF / tetrahydrofuran

4: 83 percent / Cs₂CO₃ / acetonitrile / 50 °C

5: 95 percent / Ph₃P; DEAD / tetrahydrofuran

6: 64 percent / aq. MeNH₂ / tetrahydrofuran

7: 85 percent / dimethylformamide

8: 70 percent / aq. NaOH / ethanol

9: benzotriazol-1-yloxytri(dimethylamino)phosphonium*PF₆^(1-); dimethylaminomethyl-polystyrene resin; Et₃N / CH₂Cl₂

With sodium hydroxide; oxalyl dichloride; dimethylaminomethyl-polystyrene resin; tetrabutyl ammonium fluoride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; magnesium; triethylamine; N,N-dimethyl-formamide; triphenylphosphine; methylamine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 5: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2004.05.002

Reference yield:

: 245116-17-0
3-chloro-5-hydroxy-benzoic acid benzyl ester

: 245116-23-8
C₃₃H₄₅ClN₄O₇

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / Cs₂CO₃ / acetonitrile / 50 °C

2: 95 percent / Ph₃P; DEAD / tetrahydrofuran

3: 64 percent / aq. MeNH₂ / tetrahydrofuran

4: 85 percent / dimethylformamide

5: 70 percent / aq. NaOH / ethanol

6: benzotriazol-1-yloxytri(dimethylamino)phosphonium*PF₆^(1-); dimethylaminomethyl-polystyrene resin; Et₃N / CH₂Cl₂

With sodium hydroxide; dimethylaminomethyl-polystyrene resin; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; caesium carbonate; triethylamine; triphenylphosphine; methylamine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2004.05.002