3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane

Base Information

Chemical Name:3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane
CAS No.:66958-33-6
Molecular Formula:C₄₈H₇₆O₇
Molecular Weight:765.127
Hs Code.:

3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane

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Chemical Property of 3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane

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Technology Process of 3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane

There total 1 articles about 3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-((2E,6E,10E,14E,18E,22E)-3,7,11,15,19,23,27-Heptamethyl-octacosa-2,6,10,14,18,22,26-heptaenyl)-3,4-dimethoxy-2,5-bis-methoxymethoxy-6-methyl-benzene

: 66958-33-6
3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane

Guidance literature:: With sodium hydroxide; N-Bromosuccinimide; Multistep reaction; 1) aq. 1,2-dimethoxyethane, -5 deg C, 1 h; 2) methanol, room tempearture;

Reference yield:

: 66958-33-6
3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane

: 66958-34-7
(6E,10E,14E,18E,22E,26E)-28-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-2,6,10,14,18,22,26-heptamethyl-octacosa-1,6,10,14,18,22,26-heptaen-3-ol

Guidance literature:: With aluminum isopropoxide; In toluene; for 20h; Heating;

Reference yield:

: 66958-33-6
3-[(3E,7E,11E,15E,19E,23E)-25-(3,4-Dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-3,7,11,15,19,23-hexamethyl-pentacosa-3,7,11,15,19,23-hexaenyl]-2,2-dimethyl-oxirane

: 64634-91-9
1-[(2E,6E,10E,14E,18E,22E,26E,30E,34E)-3,7,11,15,19,23,27,31,35,39-decamethyltetraconta-2,6,10,14,18,22,26,30,34,38-decaen-1-yl]-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: lithium diisopropyl amide / tetrahydrofuran

2: thionyl chloride / tetrahydrofuran; dichloromethane

3: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane

4: lithium; ethylamine

With n-butyllithium; thionyl chloride; lithium; ethylamine; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; dichloromethane;