Technology Process of C35H43N5O5
There total 8 articles about C35H43N5O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diethylamine;
In
dichloromethane;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: chloroformic acid ethyl ester; 4-methyl-morpholine / tetrahydrofuran / 0.33 h / -20 °C
1.2: 0.33 h / 0 - 5 °C
2.1: trifluoroacetic anhydride; pyridine / 3 h / 20 °C
3.1: hydroxylamine hydrochloride; potassium carbonate / ethanol / 2 h / 90 °C
4.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 3 h / 0 °C
4.2: 12 h / 20 °C
4.3: 2 h / 90 °C
5.1: diethylamine / dichloromethane / 0.5 h / 20 °C
With
4-methyl-morpholine; pyridine; hydroxylamine hydrochloride; chloroformic acid ethyl ester; potassium carbonate; diethylamine; trifluoroacetic anhydride; (bis-(2-methoxyethyl)amino)sulfur trufluoride;
In
tetrahydrofuran; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic anhydride; pyridine / 3 h / 20 °C
2.1: hydroxylamine hydrochloride; potassium carbonate / ethanol / 2 h / 90 °C
3.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 3 h / 0 °C
3.2: 12 h / 20 °C
3.3: 2 h / 90 °C
4.1: diethylamine / dichloromethane / 0.5 h / 20 °C
With
pyridine; hydroxylamine hydrochloride; potassium carbonate; diethylamine; trifluoroacetic anhydride; (bis-(2-methoxyethyl)amino)sulfur trufluoride;
In
ethanol; dichloromethane;