trans-4-cyclohexyl-4-methoxybenzoat

Base Information

Chemical Name:trans-4-cyclohexyl-4-methoxybenzoat
CAS No.:110568-52-0
Molecular Formula:C₂₉H₄₄O₃
Molecular Weight:440.667
Hs Code.:

trans-4-<trans-4-(trans-4-Propylcyclohexyl)cyclohexyl>cyclohexyl-4-methoxybenzoat

Synonyms:

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Chemical Property of trans-4-cyclohexyl-4-methoxybenzoat

Chemical Property:

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Technology Process of trans-4-cyclohexyl-4-methoxybenzoat

There total 12 articles about trans-4-cyclohexyl-4-methoxybenzoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82832-73-3
4-(trans-4-n-propylcyclohexyl)cyclohexanone

: 110568-52-0
trans-4-cyclohexyl-4-methoxybenzoat

Guidance literature:: Multi-step reaction with 13 steps

1: ethyl acetate / 0.5 h / Ambient temperature

2: 35 percent H₂O₂ / ethyl acetate; tetrahydrofuran / 1 h / Ambient temperature

3: 72 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

4: 83 percent / tert-butylhydroperoxide, VO(acac)2 / benzene / 48 h / 40 °C

5: 99 percent / CrO₃, pyridine / CH₂Cl₂ / 0.25 h / Ambient temperature

6: 66 percent / hydrazin hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature

7: 88 percent / 4-methylmorpholine / diethyl ether / 20 h / Ambient temperature

8: 91 percent / lithium iodide hydrate / dimethylformamide / 1 h / Heating

9: 94 percent / H₂ / Pt-oxide / ethyl acetate / 1 h

10: 83 percent / K₂CO₃ / diethyl ether / 16 h / Ambient temperature

11: 95 percent / 2) HCl (5 percent) / benzene / 1) 6 h, 60 deg C; 2) 30 min, r.t.

12: 55 percent / 2 N NaOH / benzene / 3 h / Heating

13: pyridine / 3 h / Ambient temperature

With 4-methyl-morpholine; pyridine; chromium(VI) oxide; hydrogenchloride; tert.-butylhydroperoxide; sodium hydroxide; lithium aluminium tetrahydride; bis(acetylacetonate)oxovanadium; hydrogen; dihydrogen peroxide; potassium carbonate; hydrazine hydrate; acetic acid; lithium iodide; Pt-oxide; In tetrahydrofuran; pyridine; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene;

Reference yield:

: 110568-42-8
(RS)-(1l,2l,3u,4u)-2,3-Epoxy-4-(trans-4-propylcyclohexyl)cyclohexanol

: 110568-52-0
trans-4-cyclohexyl-4-methoxybenzoat

Guidance literature:: Multi-step reaction with 9 steps

1: 99 percent / CrO₃, pyridine / CH₂Cl₂ / 0.25 h / Ambient temperature

2: 66 percent / hydrazin hydrate, glacial acetic acid / ethanol / 1.5 h / Ambient temperature

3: 88 percent / 4-methylmorpholine / diethyl ether / 20 h / Ambient temperature

4: 91 percent / lithium iodide hydrate / dimethylformamide / 1 h / Heating

5: 94 percent / H₂ / Pt-oxide / ethyl acetate / 1 h

6: 83 percent / K₂CO₃ / diethyl ether / 16 h / Ambient temperature

7: 95 percent / 2) HCl (5 percent) / benzene / 1) 6 h, 60 deg C; 2) 30 min, r.t.

8: 55 percent / 2 N NaOH / benzene / 3 h / Heating

9: pyridine / 3 h / Ambient temperature

With 4-methyl-morpholine; pyridine; chromium(VI) oxide; hydrogenchloride; sodium hydroxide; hydrogen; potassium carbonate; hydrazine hydrate; acetic acid; lithium iodide; Pt-oxide; In pyridine; diethyl ether; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene;

Reference yield:

: 110568-44-0
6-(trans-4-Propylcyclohexyl)-2-cyclohexen-1-ol

: 110568-52-0
trans-4-cyclohexyl-4-methoxybenzoat

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / 4-methylmorpholine / diethyl ether / 20 h / Ambient temperature

2: 91 percent / lithium iodide hydrate / dimethylformamide / 1 h / Heating

3: 94 percent / H₂ / Pt-oxide / ethyl acetate / 1 h

4: 83 percent / K₂CO₃ / diethyl ether / 16 h / Ambient temperature

5: 95 percent / 2) HCl (5 percent) / benzene / 1) 6 h, 60 deg C; 2) 30 min, r.t.

6: 55 percent / 2 N NaOH / benzene / 3 h / Heating

7: pyridine / 3 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; hydrogen; potassium carbonate; lithium iodide; Pt-oxide; In pyridine; diethyl ether; ethyl acetate; N,N-dimethyl-formamide; benzene;