4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole

Base Information

Chemical Name:4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole
CAS No.:122293-32-7
Molecular Formula:C₁₇H₂₆BNSi
Molecular Weight:283.297
Hs Code.:

Synonyms:

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Chemical Property of 4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole

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Technology Process of 4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole

There total 1 articles about 4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 81620-70-4
4,5-diethyl-2,5-dihydro-3-isopropenyl-1,2,2-trimethyl-1,2,5-azasilaborole

: 62-53-3
aniline

: 122293-32-7
4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole

Guidance literature:: In neat (no solvent); byproducts: CH3NH2; the 1-phenyl-azasilaborole reacts with aniline at 170°C (7 h); removing volitiles (< 60° C, 0.001 Torr); elem. anal.;

Reference yield:

: 15321-51-4
diiron nonacarbonyl

: 122293-32-7
4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole

: 122312-92-9
tricarbonyl(η4-4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole)iron

: 122293-49-6
tricarbonyl(η4-4,5-diethyl-2,5-dihydro-3-isopropenyl-2,2-dimethyl-1-phenyl-1H-1,2,5-azasilaborole)iron

Guidance literature:: In 1,2,5-trimethyl-benzene; byproducts: CO; (Ar); heating of azasilaborole and Fe complex in mesitylene for 4 h at 160°C; filtered soln. was concd. in vac., residue was distd. at 105-115°C/0,001 Torr, yielding mixt. of 2 isomers 95:5%; elem. anal.;