4H-Indol-4-one, 1,5,6,7-tetrahydro-3-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)-2 ,6,6-trimethyl-1-(phenylmethyl)-

Base Information

Chemical Name:4H-Indol-4-one, 1,5,6,7-tetrahydro-3-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)-2 ,6,6-trimethyl-1-(phenylmethyl)-
CAS No.:123271-69-2
Molecular Formula:C₂₆H₃₁NO₃
Molecular Weight:405.537
Hs Code.:
Mol file:123271-69-2.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4H-Indol-4-one, 1,5,6,7-tetrahydro-3-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)-2 ,6,6-trimethyl-1-(phenylmethyl)-

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Technology Process of 4H-Indol-4-one, 1,5,6,7-tetrahydro-3-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)-2 ,6,6-trimethyl-1-(phenylmethyl)-

There total 2 articles about 4H-Indol-4-one, 1,5,6,7-tetrahydro-3-(2-hydroxy-4,4-dimethyl-6-oxo-1-cyclohexen-1-yl)-2 ,6,6-trimethyl-1-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 22381-59-5
1,1-Bis-<2-hydroxy-4,4-dimethyl-6-oxo-cyclohexenyl>-2-oxo-propan

: 100-46-9
benzylamine

: 123271-69-2
1-Benzyl-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-2,6,6-trimethyl-1,5,6,7-tetrahydro-indol-4-one

: 123272-14-0
1-Benzyl-3-(2-benzylamino-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-2,6,6-trimethyl-1,5,6,7-tetrahydro-indol-4-one

Guidance literature:: In chlorobenzene; for 3h; Heating;

Reference yield:

: 126-81-8
dimedone

: 123271-69-2
1-Benzyl-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-2,6,6-trimethyl-1,5,6,7-tetrahydro-indol-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / anhyd. K₂CO₃ / CHCl₃ / 18 h / 28 °C

2: 80 percent / chlorobenzene / 3 h / Heating

With potassium carbonate; In chloroform; chlorobenzene;