2,5-Bis(11-carboxyundecyl)-3-nitro-1,4-benzochinon

Base Information

Chemical Name:2,5-Bis(11-carboxyundecyl)-3-nitro-1,4-benzochinon
CAS No.:77798-66-4
Molecular Formula:C₃₀H₄₇NO₈
Molecular Weight:549.705
Hs Code.:

Synonyms:

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Chemical Property of 2,5-Bis(11-carboxyundecyl)-3-nitro-1,4-benzochinon

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Technology Process of 2,5-Bis(11-carboxyundecyl)-3-nitro-1,4-benzochinon

There total 6 articles about 2,5-Bis(11-carboxyundecyl)-3-nitro-1,4-benzochinon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 77798-61-9
2,5-Bis(11-carboxyundecyl)hydrochinon-diacetat

: 77798-66-4
2,5-Bis(11-carboxyundecyl)-3-nitro-1,4-benzochinon

Guidance literature:: With nitric acid; In acetic anhydride; for 14h; Ambient temperature;

Reference yield:

: 1108-58-3
<10-(Methoxycarbonyl)decyl>triphenylphosphoniumiodid

: 77798-66-4
2,5-Bis(11-carboxyundecyl)-3-nitro-1,4-benzochinon

Guidance literature:: Multi-step reaction with 6 steps

1: NaOMe / dimethylformamide / 1) 0 deg C, 10 min, 2) r.t., 1.5 h

2: 70 percent / dimethylformamide / 3 h / Ambient temperature

3: 90 percent / H₂ / Raney-Ni / methanol / 5 h / 70 °C / 44130.5 Torr

4: 48percent HBr / acetic acid / 14 h / 110 °C

5: pyridine / 14 h / Ambient temperature

6: 61 percent / conc. HNO₃ / acetic anhydride / 14 h / Ambient temperature

With hydrogen bromide; hydrogen; nitric acid; sodium methylate; nickel; In pyridine; methanol; acetic anhydride; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 77798-57-3
2,5-Bis(11-methoxycarbonyl-1-undecenyl)hydrochinon-dimethylether

: 77798-66-4
2,5-Bis(11-carboxyundecyl)-3-nitro-1,4-benzochinon

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / H₂ / Raney-Ni / methanol / 5 h / 70 °C / 44130.5 Torr

2: 48percent HBr / acetic acid / 14 h / 110 °C

3: pyridine / 14 h / Ambient temperature

4: 61 percent / conc. HNO₃ / acetic anhydride / 14 h / Ambient temperature

With hydrogen bromide; hydrogen; nitric acid; nickel; In pyridine; methanol; acetic anhydride; acetic acid;