Technology Process of C34H38N2O8S
There total 6 articles about C34H38N2O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Lawessons reagent;
In
tetrahydrofuran;
at 60 ℃;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/adsc.201301112
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium azide / N,N-dimethyl-formamide / 70 °C
2.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 35 °C
3.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.75 h / -15 °C / Schlenk technique; Inert atmosphere
3.2: 2 h / 20 °C / Schlenk technique; Inert atmosphere
4.1: pyridine / dichloromethane / 0 - 20 °C / Schlenk technique; Inert atmosphere
5.1: Lawessons reagent / tetrahydrofuran / 60 °C / Schlenk technique; Inert atmosphere
With
Lawessons reagent; 4-methyl-morpholine; pyridine; lithium aluminium tetrahydride; sodium azide; isobutyl chloroformate;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201301112
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 35 °C
2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.75 h / -15 °C / Schlenk technique; Inert atmosphere
2.2: 2 h / 20 °C / Schlenk technique; Inert atmosphere
3.1: pyridine / dichloromethane / 0 - 20 °C / Schlenk technique; Inert atmosphere
4.1: Lawessons reagent / tetrahydrofuran / 60 °C / Schlenk technique; Inert atmosphere
With
Lawessons reagent; 4-methyl-morpholine; pyridine; lithium aluminium tetrahydride; isobutyl chloroformate;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/adsc.201301112