Mo(N(2,6-i-Pr2C6H3))2(N,N-di(pyrrolyl-α-methyl)-N-methylamine dianion)

Base Information

• Chemical Name: Mo(N(2,6-i-Pr2C6H3))2(N,N-di(pyrrolyl-α-methyl)-N-methylamine dianion)
• CAS No.: 720665-67-8
• Molecular Formula: C₃₅H₄₇MoN₅
• Molecular Weight: 633.732

Synonyms:

Chemical Property of Mo(N(2,6-i-Pr2C6H3))2(N,N-di(pyrrolyl-α-methyl)-N-methylamine dianion)

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Technology Process of Mo(N(2,6-i-Pr2C6H3))2(N,N-di(pyrrolyl-α-methyl)-N-methylamine dianion)

There total 1 articles about Mo(N(2,6-i-Pr2C6H3))2(N,N-di(pyrrolyl-α-methyl)-N-methylamine dianion) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

MoCl2(N(2,6-i-Pr2C6H3))2(1,2-dimethoxyethane) + N,N-di(pyrrolyl-α-methyl)-N-methylamine dilithium salt → Mo(N(2,6-i-Pr2C6H3))2(N,N-di(pyrrolyl-α-methyl)-N-methylamine dianion) (720665-67-8)

Guidance literature:

In diethyl ether; byproducts: LiCl; under N2; soln. of Li salt of ligand in ether cooled to near frozen (liq. N2); added to cold soln. of Mo complex (molar ratio 1:1) in ether; warmed to ambient temp.; stirred overnight; filtered; solvent removed in vac.; recrystd. from ether-pentane; elem. anal.;

DOI:10.1021/ic049644o

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