<3S(3α,3aα,9aα,9bβ)>-3a,6-dimethyl-3-hydroxy-1,2,3,3a,4,5,8,9,9a,9b-decahydro-7H-benzinden-7-one benzoate

Base Information

Chemical Name:<3S(3α,3aα,9aα,9bβ)>-3a,6-dimethyl-3-hydroxy-1,2,3,3a,4,5,8,9,9a,9b-decahydro-7H-benzinden-7-one benzoate
CAS No.:36031-31-9
Molecular Formula:C₂₂H₂₆O₃
Molecular Weight:338.447
Hs Code.:

<3S(3α,3aα,9aα,9bβ)>-3a,6-dimethyl-3-hydroxy-1,2,3,3a,4,5,8,9,9a,9b-decahydro-7H-benz<e>inden-7-one benzoate

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Chemical Property of <3S(3α,3aα,9aα,9bβ)>-3a,6-dimethyl-3-hydroxy-1,2,3,3a,4,5,8,9,9a,9b-decahydro-7H-benzinden-7-one benzoate

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Technology Process of <3S(3α,3aα,9aα,9bβ)>-3a,6-dimethyl-3-hydroxy-1,2,3,3a,4,5,8,9,9a,9b-decahydro-7H-benzinden-7-one benzoate

There total 2 articles about <3S(3α,3aα,9aα,9bβ)>-3a,6-dimethyl-3-hydroxy-1,2,3,3a,4,5,8,9,9a,9b-decahydro-7H-benzinden-7-one benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Benzoic acid (3S,3aS,9aS,9bS)-3a-methyl-7-oxo-6-phenylsulfanylmethyl-2,3,3a,4,5,7,8,9,9a,9b-decahydro-1H-cyclopenta[a]naphthalen-3-yl ester

: 36031-31-9
<3S(3α,3aα,9aα,9bβ)>-3a,6-dimethyl-3-hydroxy-1,2,3,3a,4,5,8,9,9a,9b-decahydro-7H-benzinden-7-one benzoate

Guidance literature:: With nickel; In acetone; for 5h; Yield given; Heating;
DOI:10.1021/jm00150a009

Reference yield:

: 23477-71-6
3β-Benzoyloxy-3aβ-methyl-7-oxo-2.3.3a.4.5.7.8.9.9aβ.9bα-decahydro-1H-cyclopenta naphthalin

: 36031-31-9
<3S(3α,3aα,9aα,9bβ)>-3a,6-dimethyl-3-hydroxy-1,2,3,3a,4,5,8,9,9a,9b-decahydro-7H-benzinden-7-one benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.43 g / triethanolamine / H₂O / 16 h / Heating

2: Raney nickel / acetone / 5 h / Heating

With triethanolamine; nickel; In water; acetone;
DOI:10.1021/jm00150a009