5-methyl-trans-1,3-cyclohexanediol

Base Information

• Chemical Name: 5-methyl-trans-1,3-cyclohexanediol
• CAS No.: 33941-95-6
• Molecular Formula: C₇H₁₄O₂
• Molecular Weight: 130.187
• Mol file: 33941-95-6.mol

Synonyms:

Chemical Property of 5-methyl-trans-1,3-cyclohexanediol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-methyl-trans-1,3-cyclohexanediol

There total 4 articles about 5-methyl-trans-1,3-cyclohexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

orcinol (504-15-4) → 5-methyl-trans-1,3-cyclohexanediol (33941-95-6,54773-78-3,54773-79-4)

Guidance literature:

With hydrogen; rhodium on alumina; In methanol;

DOI:10.1021/ja00745a022

Reference yield:

orcinol (504-15-4) → cis-5-methyl-cis-1,3-cyclohexanediol (54773-78-3) + trans-5-methyl-cis-1,3-cyclohexanediol (54773-79-4) + 5-methyl-trans-1,3-cyclohexanediol (33941-95-6,54773-78-3,54773-79-4)

Guidance literature:

With hydrogen; sodium ethanolate; nickel; In ethanol; at 130 - 160 ℃; under 76000.1 - 91200.1 Torr; Yields of byproduct given;

DOI:10.1016/S0040-4020(01)98859-3

Reference yield:

5-methylcyclohexan-1,3-dione (4341-24-6) → cis-5-methyl-cis-1,3-cyclohexanediol (54773-78-3) + trans-5-methyl-cis-1,3-cyclohexanediol (54773-79-4) + 5-methyl-trans-1,3-cyclohexanediol (33941-95-6,54773-78-3,54773-79-4)

Guidance literature:

With isopropyl alcohol; ruthenium-based catalyst; In toluene; at 120 ℃; for 2h; Title compound not separated from byproducts; microwave irradiation;

DOI:10.1021/jo0612527

upstream raw materials:

orcinol

5-methylcyclohexan-1,3-dione

Downstream raw materials:

DL-trans-3,5-Dimethoxy-methylcyclohexan

5-Chloro-3-methyl-cyclohexene

r-1,t-3-dichloro-5-methylcyclohexane

r-1,c-3-dichloro-t-5-methyl cyclohexane