dimethyl (2R,3R,3aR,6aR,9R,12aR)-9,12a-dimethyl-2,6-(13-isopropyletheno)-5-(phenylamino)-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate

Base Information

• Chemical Name: dimethyl (2R,3R,3aR,6aR,9R,12aR)-9,12a-dimethyl-2,6-(13-isopropyletheno)-5-(phenylamino)-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate
• CAS No.: 1160170-68-2
• Molecular Formula: C₃₂H₄₂N₂O₄
• Molecular Weight: 518.696

Synonyms:

Chemical Property of dimethyl (2R,3R,3aR,6aR,9R,12aR)-9,12a-dimethyl-2,6-(13-isopropyletheno)-5-(phenylamino)-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate

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Technology Process of dimethyl (2R,3R,3aR,6aR,9R,12aR)-9,12a-dimethyl-2,6-(13-isopropyletheno)-5-(phenylamino)-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate

There total 2 articles about dimethyl (2R,3R,3aR,6aR,9R,12aR)-9,12a-dimethyl-2,6-(13-isopropyletheno)-5-(phenylamino)-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

dimethyl (1R,4aR,7R,8R,11aR)-1,4a-dimethyl-6,8a-(11-isopropyletheno)-8-(3-phenylureido)tetradecahydrophenanthrene-1,7-dicarboxylate → dimethyl (2R,3R,3aR,6aR,9R,12aR)-9,12a-dimethyl-2,6-(13-isopropyletheno)-5-(phenylamino)-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate (1160170-68-2)

Guidance literature:

With trichlorophosphate; In toluene; for 0.5h; Reflux;

DOI:10.1134/S0012500808110098

Reference yield:

C32H44N2O5 (1160170-66-0) → dimethyl (2R,3R,3aR,6aR,9R,12aR)-9,12a-dimethyl-2,6-(13-isopropyletheno)-5-(phenylamino)-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate (1160170-68-2)

Guidance literature:

With trichlorophosphate;

DOI:10.1134/S1070428010080051

Reference yield: 57.0%

dimethyl (2R,3R,3aR,6aR,9R,12aR)-9,12a-dimethyl-2,6-(13-isopropyletheno)-5-(phenylamino)-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate (1160170-68-2) + p-toluenesulfonyl chloride (98-59-9) → dimethyl (2S,3R,3aR,6aS,9R,12aR)-2,6-(isopropylidenemethano)-9,12a-dimethyl-5-[(4-methylphenylsulfonyl)(phenyl)amino]-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate (1253976-26-9)

Guidance literature:

With triethylamine; In chloroform; for 18h;

DOI:10.1134/S1070428010080051

upstream raw materials:

C₃₂H₄₄N₂O₅

Downstream raw materials:

dimethyl (2S,3R,3aR,6aS,9R,12aR)-2,6-(isopropylidenemethano)-9,12a-dimethyl-5-[(4-methylphenylsulfonyl)(phenyl)amino]-1,2,3,3a,6,7,8,8a,9,10,11,12,12a,12b-tetradecahydronaphtho[2,1-d]indole-3,9-dicarboxylate

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