N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid

Base Information

Chemical Name:N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid
CAS No.:86041-02-3
Molecular Formula:C₅₁H₆₈N₄O₁₅P*Cl
Molecular Weight:1043.55
Hs Code.:

N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid

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Chemical Property of N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid

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Technology Process of N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid

There total 5 articles about N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 61083-76-9
N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucin-chlorid

: 86041-00-1
Leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester

: 86041-02-3
N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid

Guidance literature:: With N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane; 1) 2 h, -15 deg C, 2) 56 h, room temperature;
DOI:10.1002/jlac.198319830303

Reference yield:

: 25644-83-1
O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-N-(benzyloxycarbonyl)serin-methylester

: 86041-02-3
N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / H₂ / 10percent Pd/C / methanol / 3 h / Ambient temperature

2: 74 percent / (ethyl)-2-ethoxy-1,2-dihydro-1-quinolinecarboxylate / CHCl₃ / 1) 1 h, -15 deg C, 2) room temperature, 15 h

3: 76 percent / morpholine / CH₂Cl₂ / 0.33 h / Ambient temperature

4: 60 percent / (ethyl)-2-ethoxy-1,2-dihydro-1-quinolinecarboxylate / CH₂Cl₂ / 1) 2 h, -15 deg C, 2) 56 h, room temperature

With morpholine; hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; palladium on activated charcoal; In methanol; dichloromethane; chloroform;
DOI:10.1002/jlac.198319830303

Reference yield:

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 86041-02-3
N-<2-(Triphenylphosphonio)ethoxycarbonyl>leucyl-leucyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid

Guidance literature:: Multi-step reaction with 5 steps

1: 30 percent / Hg(CN)2 / benzene

2: 94 percent / H₂ / 10percent Pd/C / methanol / 3 h / Ambient temperature

3: 74 percent / (ethyl)-2-ethoxy-1,2-dihydro-1-quinolinecarboxylate / CHCl₃ / 1) 1 h, -15 deg C, 2) room temperature, 15 h

4: 76 percent / morpholine / CH₂Cl₂ / 0.33 h / Ambient temperature

5: 60 percent / (ethyl)-2-ethoxy-1,2-dihydro-1-quinolinecarboxylate / CH₂Cl₂ / 1) 2 h, -15 deg C, 2) 56 h, room temperature

With morpholine; hydrogen; mercury(II) cyanide; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; palladium on activated charcoal; In methanol; dichloromethane; chloroform; benzene;
DOI:10.1002/jlac.198319830303