2,3,4,6-Tetra-O-benzyl-1-C--D-xylo-5-hexosulose

Base Information

Chemical Name:2,3,4,6-Tetra-O-benzyl-1-C--D-xylo-5-hexosulose
CAS No.:140658-51-1
Molecular Formula:C₃₇H₄₀O₆S₂
Molecular Weight:644.853
Hs Code.:

2,3,4,6-Tetra-O-benzyl-1-C-<bis(methylthio)methyl>-D-xylo-5-hexosulose

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,4,6-Tetra-O-benzyl-1-C--D-xylo-5-hexosulose

Chemical Property:

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Technology Process of 2,3,4,6-Tetra-O-benzyl-1-C--D-xylo-5-hexosulose

There total 1 articles about 2,3,4,6-Tetra-O-benzyl-1-C--D-xylo-5-hexosulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116308-10-2,116308-11-3
2,3,4,6-Tetra-O-benzyl-1-C--D-glucitol

: 140658-51-1
2,3,4,6-Tetra-O-benzyl-1-C--D-xylo-5-hexosulose

Guidance literature:: With dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; Yield given. Multistep reaction; 1) CH₂Cl₂, -70 to -65 deg C, 1 h, 2) CH₂Cl₂, -70 to -65 deg C, 15 min;
DOI:10.1021/jo00039a025

Reference yield:

: 140658-51-1
2,3,4,6-Tetra-O-benzyl-1-C--D-xylo-5-hexosulose

: 116308-20-4
(1S)-(1(OH),2,4/1,3)-2,3,4-Tri-O-benzyl-1-C-<(benzyloxy)methyl>-5-oxo-6,6-bis(methylthio)-1,2,3,4-cyclohexanetetrol

Guidance literature:: With 18-crown-6 ether; sodium acetate; In toluene; for 16h; Yield given; Ambient temperature;
DOI:10.1021/jo00039a025

Reference yield:

: 140658-51-1
2,3,4,6-Tetra-O-benzyl-1-C--D-xylo-5-hexosulose

: 116308-20-4
(1S)-(1(OH),2,4/1,3)-2,3,4-Tri-O-benzyl-1-C-<(benzyloxy)methyl>-5-oxo-6,6-bis(methylthio)-1,2,3,4-cyclohexanetetrol

: 140849-67-8
(1R)-(1(CH2OH),2,4/1,3)-2,3,4-Tri-O-benzyl-1-C-<(benzyloxy)methyl>-6,6-bis(methylthio)-5-oxo-1,2,3,4-cyclohexanetetrol

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In toluene; for 18h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00039a025