dibromobis(o-phenylenebis(diphenylphosphine))iron

Base Information

Chemical Name:dibromobis(o-phenylenebis(diphenylphosphine))iron
CAS No.:101566-86-3
Molecular Formula:C₆₀H₄₈Br₂FeP₄
Molecular Weight:1108.59
Hs Code.:

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Chemical Property of dibromobis(o-phenylenebis(diphenylphosphine))iron

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Technology Process of dibromobis(o-phenylenebis(diphenylphosphine))iron

There total 2 articles about dibromobis(o-phenylenebis(diphenylphosphine))iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 13991-08-7
o-phenylenebis(diphenylphosphine)

: 7789-46-0
iron(II) bromide

: 101566-86-3
dibromobis(o-phenylenebis(diphenylphosphine))iron

Guidance literature:: In tetrahydrofuran; under N2; FeBr2 treated with THF; taken to dryness; residue mixt with opdp and acetone; stirred for 24 h at 20°C; solid extd. with CH2Cl2 (Soxhlet);; filtration; crystals dried (1E-3 mmHg); elem. anal.;
DOI:10.1039/DT9880002865

Reference yield:

: iron(II) bromide tetrahydrate

: 13991-08-7
o-phenylenebis(diphenylphosphine)

: 101566-86-3
dibromobis(o-phenylenebis(diphenylphosphine))iron

Guidance literature:: With Fe; In ethanol; dichloromethane; refluxing FeBr2*4H2O in ethanol with iron filings; filtration into a stirred soln. of ligand in ethanol/CH2Cl2; slowly reducing of solvent volume (vac., 0°C); filtration; washing (ethanol); drying in vac.; elem. anal.;