ethyl 3-carbamoyl>acrylate

Base Information

Chemical Name:ethyl 3-carbamoyl>acrylate
CAS No.:106899-16-5
Molecular Formula:C₂₂H₂₅NO₄
Molecular Weight:367.445
Hs Code.:

ethyl 3-<N-benzyl-N-<2-(3-hydroxypropyl)phenyl>carbamoyl>acrylate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-carbamoyl>acrylate

Chemical Property:

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Technology Process of ethyl 3-carbamoyl>acrylate

There total 4 articles about ethyl 3-carbamoyl>acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 26367-48-6
fumaric acid ethyl ester mono chloride

: 106899-15-4
3-(2-Benzylamino-phenyl)-propan-1-ol

: 106899-16-5
ethyl 3-carbamoyl>acrylate

Guidance literature:: In dichloromethane;
DOI:10.1248/cpb.34.140

Reference yield:

: 1466-88-2,66894-06-2
2-nitrocinnamic aldehyde

: 106899-16-5
ethyl 3-carbamoyl>acrylate

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / NaBH₄ / methanol

2: 94 percent / hydrogen / 5 percent Pd-C / ethanol / Ambient temperature

3: 86 percent / NaBH₄ / acetic acid

4: 82 percent / CH₂Cl₂

With sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; ethanol; dichloromethane; acetic acid;
DOI:10.1248/cpb.34.140

Reference yield:

: 1504-65-0,130489-97-3
2-nitrocinnamyl alcohol

: 106899-16-5
ethyl 3-carbamoyl>acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / hydrogen / 5 percent Pd-C / ethanol / Ambient temperature

2: 86 percent / NaBH₄ / acetic acid

3: 82 percent / CH₂Cl₂

With sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane; acetic acid;
DOI:10.1248/cpb.34.140