N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

Base Information

Chemical Name:N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide
CAS No.:1452855-00-3
Molecular Formula:C₁₉H₃₀F₃NO₅S₂*C₂₃H₄₁N₃O
Molecular Weight:849.176
Hs Code.:

Synonyms:

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Chemical Property of N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

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Technology Process of N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

There total 2 articles about N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1240016-79-8
N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium chloride

: potassium {[4-(dodecyloxy)phenyl]sulfonyl}[(trifluoromethyl)sulfonyl]azanide

: 1452855-00-3
N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

Guidance literature:: In acetonitrile; for 0.0833333h; Inert atmosphere; Reflux;
DOI:10.3762/bjoc.9.121

Reference yield:

: 58076-34-9
4-(dodecyloxy)benzene-1-sulfonyl chloride

: 1452855-00-3
N-(4-(dodecyloxy)phenyl)-N',N',N'',N''-tetramethylguanidinium ((4-(dodecyloxy)phenyl)sulfonyl)((trifluoromethyl)sulfonyl)azanide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 12 h / 40 °C / Inert atmosphere

1.2: 0.08 h / 65 °C / Inert atmosphere

2.1: acetonitrile / 0.08 h / Inert atmosphere; Reflux

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.3762/bjoc.9.121