tetraphenylantimony benzenesulfonate hydrate

Base Information

Chemical Name:tetraphenylantimony benzenesulfonate hydrate
CAS No.:104316-52-1
Molecular Formula:C₃₀H₂₅O₃SSb*H₂O
Molecular Weight:605.358
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraphenylantimony benzenesulfonate hydrate

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Technology Process of tetraphenylantimony benzenesulfonate hydrate

There total 2 articles about tetraphenylantimony benzenesulfonate hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2170-05-0
pentaphenylantimony

: 7446-11-9
sulfur trioxide

: 7732-18-5
water

: 104316-52-1
tetraphenylantimony benzenesulfonate hydrate

Guidance literature:: In toluene; sulfur trioxide was passed for 7 min at 25° C througgh a solutionof pentaarylantimony in toluene; solvent was removed in a water-jet-pump vacuum; purified by recrystallization from ethanol;

Reference yield: 67.0%

: 13371-35-2,19638-16-5
tetraphenylstibonium hydroxide

: 98-11-3
benzenesulfonic acid

: 104316-52-1
tetraphenylstibonium benzenesulphonate hydrate

Guidance literature:: In methanol; byproducts: H2O; stirring (room temp., 2 h);; solvent removal (vac.), recrystn.; elem. anal.;;
DOI:10.1016/0022-328X(85)88068-2