(PS)-N⁶-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N⁶-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N⁶-benzoyl-2',3'-bis-O-.....

Base Information

• Chemical Name: (PS)-N⁶-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N⁶-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N⁶-benzoyl-2',3'-bis-O-.....
• CAS No.: 135711-72-7
• Molecular Formula: C₁₀₁H₁₂₇N₁₇O₁₈P₂S₂Si₄
• Molecular Weight: 2105.64

Synonyms:

Chemical Property of (PS)-N⁶-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N⁶-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N⁶-benzoyl-2',3'-bis-O-.....

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (PS)-N⁶-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N⁶-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N⁶-benzoyl-2',3'-bis-O-.....

There total 4 articles about (PS)-N⁶-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N⁶-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N⁶-benzoyl-2',3'-bis-O-..... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 3'-(2-Cyanoethyl N,N-Diisopropylphosphoroamidite) (135711-69-2) + (PS)-N6-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-(OP-(2-cyanoethyl)>->5')-N6-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>adenosine (135711-74-9) → (PR)-N6-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N6-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N6-benzoyl-2',3'-bis-O-..... (135711-72-7,135818-65-4,135818-66-5,135818-67-6) + (PS)-N6-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N6-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N6-benzoyl-2',3'-bis-O-..... (135711-72-7,135818-65-4,135818-66-5,135818-67-6)

Guidance literature:

With sulfur; 3-nitro-1,2,4-triazole; Yield given. Multistep reaction. Yields of byproduct given; 1) MeCN, r.t., 2 h, 2) pyridine, 20 h;

DOI:10.1002/hlca.19910740420

Reference yield:

N6-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 3'-(2-Cyanoethyl N,N-Diisopropylphosphoroamidite) (135711-69-2) + (PS)-N6-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-(OP-(2-cyanoethyl)>->5')-N6-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>adenosine (135711-74-9) → (PR)-N6-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N6-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N6-benzoyl-2',3'-bis-O-..... (135711-72-7,135818-65-4,135818-66-5,135818-67-6) + (PS)-N6-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PS)-N6-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N6-benzoyl-2',3'-bis-O-..... (135711-72-7,135818-65-4,135818-66-5,135818-67-6)

Guidance literature:

With sulfur; 3-nitro-1,2,4-triazole; Yield given. Multistep reaction. Yields of byproduct given; 1) MeCN, r.t., 2 h, 2) pyridine, 20 h;

DOI:10.1002/hlca.19910740420

Reference yield:

N6-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 3'-(2-Cyanoethyl N,N-Diisopropylphosphoroamidite) (135711-69-2) + (PR)-N6-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-N6-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>adenosine (135711-74-9) → (PR)-N6-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PR)-N6-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N6-benzoyl-2',3'-bis-O-..... (135711-72-7,135818-65-4,135818-66-5,135818-67-6) + (PS)-N6-Benzoyl-2'--5'-O-(monomethoxytrityl)-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-(PR)-N6-benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5)-N6-benzoyl-2',3'-bis-O-..... (135711-72-7,135818-65-4,135818-66-5,135818-67-6)

Guidance literature:

With sulfur; 3-nitro-1,2,4-triazole; Yield given. Multistep reaction. Yields of byproduct given; 1) MeCN, r.t., 2 h, 2) pyridine, 20 h;

DOI:10.1002/hlca.19910740420

upstream raw materials:

N⁶-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-5'-O-(monomethoxytrityl)adenosine 3'-(2-Cyanoethyl N,N-Diisopropylphosphoroamidite)

(PR)-N⁶-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-P-(2-cyanoethyl)>->5')-N⁶-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>adenosine

(PS)-N⁶-Benzoyl-2'-O-<(tert-butyl)dimethylsilyl>-P-thioadenylyl-(3'-(O^P-(2-cyanoethyl)>->5')-N⁶-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>adenosine

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