2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-1-O-acetyl-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

Base Information

Chemical Name:2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-1-O-acetyl-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose
CAS No.:120312-15-4
Molecular Formula:C₅₀H₆₀N₂O₁₄
Molecular Weight:913.031
Hs Code.:

2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-1-O-acetyl-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

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Chemical Property of 2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-1-O-acetyl-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

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Technology Process of 2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-1-O-acetyl-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

There total 5 articles about 2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-1-O-acetyl-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120312-14-3
(R)-2-[(2S,3R,4R,5S,6R)-2-Acetoxy-3-azido-5-((2R,3R,4R,5S,6R)-3-azido-4,5-bis-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-6-benzyloxymethyl-tetrahydro-pyran-4-yloxy]-propionic acid methyl ester

: 120312-15-4
Acetyl 2-acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-<(R)-1-methoxycarbonyl)ethyl>-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, AcOH / Pd-black / methanol; dioxane / 2 h / 750.06 Torr

2: 4 h

With hydrogen; acetic acid; palladium; In 1,4-dioxane; methanol;

Reference yield:

: 99049-62-4
2-azido-2-deoxy-3,4,6-tri-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 120312-15-4
2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-1-O-acetyl-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 0.1M BF₃*Et₂O / CH₂Cl₂; hexane / 8 h / -20 °C

2: 75 percent / 1M NBu₄F / tetrahydrofuran / 6 h / Ambient temperature

3: 1.) NiCl₂, H₃BO₃, NaBH₄; / 1.) CH₃OH, 5 deg C, 1h; 2.) 12 h

With sodium tetrahydroborate; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; boric acid; nickel dichloride; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 120312-11-0
tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

: 120312-15-4
2-Acetamido-4-O-(2-acetamido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-1-O-acetyl-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 1M NBu₄F / tetrahydrofuran / 6 h / Ambient temperature

2: 1.) NiCl₂, H₃BO₃, NaBH₄; / 1.) CH₃OH, 5 deg C, 1h; 2.) 12 h

With sodium tetrahydroborate; tetrabutyl ammonium fluoride; boric acid; nickel dichloride; In tetrahydrofuran;