C₂₅H₃₂N₂O₆*C₂HF₃O₂

Base Information

Chemical Name:C₂₅H₃₂N₂O₆*C₂HF₃O₂
CAS No.:1584664-46-9
Molecular Formula:C₂HF₃O₂*C₂₅H₃₂N₂O₆
Molecular Weight:570.563
Hs Code.:

C<sub>25</sub>H<sub>32</sub>N<sub>2</sub>O<sub>6</sub>*C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>

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Chemical Property of C₂₅H₃₂N₂O₆*C₂HF₃O₂

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Technology Process of C₂₅H₃₂N₂O₆*C₂HF₃O₂

There total 8 articles about C₂₅H₃₂N₂O₆*C₂HF₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872369-20-5
C₁₅H₃₂O₃Si

: 1584664-46-9
C₂₅H₃₂N₂O₆*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: pyridine hydrogenfluoride / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 8 h / 20 °C / Inert atmosphere

4: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With dmap; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2014.01.004

Reference yield:

: 1464823-37-7
(2R,3S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(benzyloxy)-3-hydroxy-2-methylpentan-1-one

: 1584664-46-9
C₂₅H₃₂N₂O₆*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 9 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Inert atmosphere; Cooling

2: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C / Inert atmosphere

3: n-butyllithium / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

4: hydrogen; palladium 10% on activated carbon / ethanol / 12 h

5: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 3 h / 20 °C / Inert atmosphere

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

7: pyridine hydrogenfluoride / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

8: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 8 h / 20 °C / Inert atmosphere

9: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With dmap; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; acetonitrile; 3: |Wittig Olefination;
DOI:10.1016/j.tetasy.2014.01.004

Reference yield:

: 1584664-36-7
(2R,3S)-1-((S)-4-benzyl-2-thioxothiazolidin-3-yl)-5-(benzyloxy)-3-(tert-butyldimethylsilyloxy)-2-methylpentan-1-one

: 1584664-46-9
C₂₅H₃₂N₂O₆*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 8 steps

1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C / Inert atmosphere

2: n-butyllithium / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

3: hydrogen; palladium 10% on activated carbon / ethanol / 12 h

4: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / 3 h / 20 °C / Inert atmosphere

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

6: pyridine hydrogenfluoride / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

7: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 8 h / 20 °C / Inert atmosphere

8: dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

With dmap; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; acetonitrile; 2: |Wittig Olefination;
DOI:10.1016/j.tetasy.2014.01.004