trans-N-tosyl perhydro 1H-indole-2-carboxylique

Base Information

Chemical Name:trans-N-tosyl perhydro 1H-indole-2-carboxylique
CAS No.:134786-37-1
Molecular Formula:C₁₆H₂₁NO₄S
Molecular Weight:323.413
Hs Code.:

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Chemical Property of trans-N-tosyl perhydro 1H-indole-2-carboxylique

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Technology Process of trans-N-tosyl perhydro 1H-indole-2-carboxylique

There total 23 articles about trans-N-tosyl perhydro 1H-indole-2-carboxylique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 134786-23-5,134786-24-6,134786-25-7,134786-26-8
(+/-)-(cis-1-tosyloctahydro-1H-indol-2-yl)methanol

: 134786-37-1,134786-38-2,134786-39-3,134820-89-6
cis-1-tosyloctahydro-1H-indole-2-carboxylic acid

Guidance literature:: With chromium(VI) oxide; sulfuric acid; water; In acetone; a) -5 deg C, 3 h, b) room temperature, 5 h;
DOI:10.1016/S0040-4020(01)96036-3

Reference yield: 85.0%

: 134786-23-5,134786-24-6,134786-25-7,134786-26-8
(+/-)-(trans-1-tosyloctahydro-1H-indol-2-yl)methanol

: 134786-37-1,134786-38-2,134786-39-3,134820-89-6
trans-N-tosyl perhydro 1H-indole-2-carboxylique

Guidance literature:: With chromium(VI) oxide; sulfuric acid; water; In acetone; a) -5 deg C, 3 h, b) room temperature, 5 h;
DOI:10.1016/S0040-4020(01)96036-3

Reference yield: 67.0%

: rac-(2R,3aR,7aR)-2-phenyl-1-tosyloctahydro-1H-indole

: 134786-37-1,134786-38-2,134786-39-3,134820-89-6
cis-1-tosyloctahydro-1H-indole-2-carboxylic acid

Guidance literature:: rac-(2R,3aR,7aR)-2-phenyl-1-tosyloctahydro-1H-indole; With tetrachloromethane; sodium periodate; In water; acetonitrile; at 20 ℃; for 0.25h;

With ruthenium trichloride; In water; acetonitrile; at 20 ℃; for 10h;
DOI:10.1039/c7ob00528h