1,6-Di--hexa-1,5-diin

Base Information

Chemical Name:1,6-Di--hexa-1,5-diin
CAS No.:71313-57-0
Molecular Formula:C₁₈H₂₂
Molecular Weight:238.373
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-Di--hexa-1,5-diin

Chemical Property:

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Technology Process of 1,6-Di--hexa-1,5-diin

There total 4 articles about 1,6-Di--hexa-1,5-diin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 67546-62-7
1-bromo-3-(cyclohex-1-enyl)-2-propyne

: 63768-73-0
cyclohexene-1 yle-3 propadiene-1,2

: 1655-05-6
1-(1-propynyl)cyclohexene

: 71313-57-0
1,6-Di--hexa-1,5-diin

: 71313-58-1
1,4-Di--hexa-4,5-dien-1-in

Guidance literature:: With lithium aluminium tetrahydride; copper(I) bromide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 0 ℃;

Reference yield: 9.0%

: 71313-48-9
3-(cyclohex-1-en-1-yl)prop-2-yn-1-yl 4-methylbenzenesulfonate

: 63768-73-0
cyclohexene-1 yle-3 propadiene-1,2

: 1655-05-6
1-(1-propynyl)cyclohexene

: 67546-62-7
1-bromo-3-(cyclohex-1-enyl)-2-propyne

: 71313-57-0
1,6-Di--hexa-1,5-diin

: 71313-58-1
1,4-Di--hexa-4,5-dien-1-in

Guidance literature:: With lithium aluminium tetrahydride; copper(I) bromide; In tetrahydrofuran; at 0 ℃; for 1.25h; Product distribution; Mechanism; further temperatures, reagents, solvents;

Reference yield:

: 71313-48-9
3-(cyclohex-1-en-1-yl)prop-2-yn-1-yl 4-methylbenzenesulfonate

: 71313-57-0
1,6-Di--hexa-1,5-diin

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / MgBr₂ / diethyl ether / 0 °C

2: LiAlH₄, CuBr / tetrahydrofuran; hexamethylphosphoric acid triamide / 0 °C

With lithium aluminium tetrahydride; copper(I) bromide; magnesium bromide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;